1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(phenyl(phenylsulfonyl)methyl)carbamate

Base Information

Chemical Name:1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(phenyl(phenylsulfonyl)methyl)carbamate
CAS No.:1192350-28-9
Molecular Formula:C₂₆H₂₉NO₆S
Molecular Weight:483.585
Hs Code.:

Synonyms:1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(phenyl(phenylsulfonyl)methyl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(phenyl(phenylsulfonyl)methyl)carbamate

Chemical Property:

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Technology Process of 1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(phenyl(phenylsulfonyl)methyl)carbamate

There total 1 articles about 1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(phenyl(phenylsulfonyl)methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1192350-49-4
C₁₃H₁₉NO₄

: 873-55-2
sodium benzenesulfonate

: 100-52-7
benzaldehyde

: 1192350-28-9
1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(phenyl(phenylsulfonyl)methyl)carbamate

Guidance literature:: With chloro-trimethyl-silane; formic acid; In toluene; acetonitrile; at 50 ℃; for 24h; Inert atmosphere;
DOI:10.1002/adsc.200800798

Reference yield: 25.0%

: potassium cyanide

: 1192350-28-9
1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(phenyl(phenylsulfonyl)methyl)carbamate

: 1192350-40-5
1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(cyano(phenyl)methyl)carbamate

: 1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(cyano(phenyl)methyl)carbamate

Guidance literature:: With quinine; In dichloromethane; at -10 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/adsc.200800798

Reference yield:

: potassium cyanide

: 1192350-28-9
1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(phenyl(phenylsulfonyl)methyl)carbamate

: 71849-99-5
(+/-)-α-phenylglycine hydrochloride

Guidance literature:: potassium cyanide; 1-(3,4-dimethoxyphenyl)-2-methylpropan-2-yl N-(phenyl(phenylsulfonyl)methyl)carbamate; With quinine; In dichloromethane; at -10 ℃; for 24h; Inert atmosphere;

With hydrogenchloride; In water; at 60 ℃; for 16h;
DOI:10.1002/adsc.200800798