diethyl 4,4'-dihydroxy-5,5'-dimethoxy-8,3'-neolign-7,7'-dien-9,9'-dionate

Base Information

Chemical Name:diethyl 4,4'-dihydroxy-5,5'-dimethoxy-8,3'-neolign-7,7'-dien-9,9'-dionate
CAS No.:864668-60-0
Molecular Formula:C₂₄H₂₆O₈
Molecular Weight:442.466
Hs Code.:

Synonyms:diethyl 4,4'-dihydroxy-5,5'-dimethoxy-8,3'-neolign-7,7'-dien-9,9'-dionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 4,4'-dihydroxy-5,5'-dimethoxy-8,3'-neolign-7,7'-dien-9,9'-dionate

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Technology Process of diethyl 4,4'-dihydroxy-5,5'-dimethoxy-8,3'-neolign-7,7'-dien-9,9'-dionate

There total 2 articles about diethyl 4,4'-dihydroxy-5,5'-dimethoxy-8,3'-neolign-7,7'-dien-9,9'-dionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 28028-62-8,74257-26-4,4046-02-0
ethyl ferulate

: 864668-60-0
diethyl 4,4'-dihydroxy-5,5'-dimethoxy-8,3'-neolign-7,7'-dien-9,9'-dionate

Guidance literature:: ethyl ferulate; With potassium hydroxide; In water; benzene; for 0.166667h;

With potassium hexacyanoferrate(III); In water; benzene; for 0.5h;
DOI:10.1016/j.bmc.2013.12.067

Reference yield:

: 1135-24-6,537-98-4
3-(4-hydroxy-3-methoxyphenyl)acrylic acid

: 864668-60-0
diethyl 4,4'-dihydroxy-5,5'-dimethoxy-8,3'-neolign-7,7'-dien-9,9'-dionate

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / 2 h / 20 °C

2.1: potassium hydroxide / water; benzene / 0.17 h

2.2: 0.5 h

With thionyl chloride; potassium hydroxide; In water; benzene;
DOI:10.1016/j.bmc.2013.12.067