N-[3-(tert-butoxycarbonylamino)propyl]-N'-5-(tert-butoxycarbonylamino)-1,5-diaminopentane

Base Information

• Chemical Name: N-[3-(tert-butoxycarbonylamino)propyl]-N'-5-(tert-butoxycarbonylamino)-1,5-diaminopentane
• CAS No.: 944278-03-9
• Molecular Formula: C₁₈H₃₇N₃O₄
• Molecular Weight: 359.509

Synonyms:N-[3-(tert-butoxycarbonylamino)propyl]-N'-5-(tert-butoxycarbonylamino)-1,5-diaminopentane

Chemical Property of N-[3-(tert-butoxycarbonylamino)propyl]-N'-5-(tert-butoxycarbonylamino)-1,5-diaminopentane

Chemical Property:

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Technology Process of N-[3-(tert-butoxycarbonylamino)propyl]-N'-5-(tert-butoxycarbonylamino)-1,5-diaminopentane

There total 1 articles about N-[3-(tert-butoxycarbonylamino)propyl]-N'-5-(tert-butoxycarbonylamino)-1,5-diaminopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

5-tert-butoxycarbonylamino-1-aminopentane (51644-96-3) + 3-bromopropylamine tert-butylcarbamate (83948-53-2) → N-[3-(tert-butoxycarbonylamino)propyl]-N'-5-(tert-butoxycarbonylamino)-1,5-diaminopentane (944278-03-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

DOI:10.1016/j.bmc.2007.05.054

Reference yield: 100.0%

N-[3-(tert-butoxycarbonylamino)propyl]-N'-5-(tert-butoxycarbonylamino)-1,5-diaminopentane (944278-03-9) + 3,5-di-[3-(tert-butoxycarbonylamino)propoxy]benzyl chloride (944277-96-7) → N-[(tert-butoxycarbonylamino)propyl]-N-[5-(tert-butoxycarbonylamino)pentyl]-3,5-di[(tert-butoxycarbonylamino)propoxy]benzylamine (944278-04-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 3h;

DOI:10.1016/j.bmc.2007.05.054

Reference yield: 61.0%

3,5-dihydroxyphenol (108-73-6) + N-[3-(tert-butoxycarbonylamino)propyl]-N'-5-(tert-butoxycarbonylamino)-1,5-diaminopentane (944278-03-9) → N-[3-(tert-butoxycarbonylamino)propyl]-N-[5-(tert-butoxycarbonylamino)pentyl]-3,5-dihydroxyaniline (944278-05-1)

Guidance literature:

In tetrahydrofuran; for 2h; Heating;

DOI:10.1016/j.bmc.2007.05.054

upstream raw materials:

5-tert-butoxycarbonylamino-1-aminopentane

3-bromopropylamine tert-butylcarbamate

Downstream raw materials:

N-[(tert-butoxycarbonylamino)propyl]-N-[5-(tert-butoxycarbonylamino)pentyl]-3,5-di[(tert-butoxycarbonylamino)propoxy]benzylamine

N-[3-(tert-butoxycarbonylamino)propyl]-N-[5-(tert-butoxycarbonylamino)pentyl]-3,5-dihydroxyaniline

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