(3aS,4R,6S,6aR)-6-hydroxy-2,2-dimethyltetrahydro-3aH-cyclo-penta[d][1,3]dioxol-4-aminium (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate dibenzoyl-L-tartrate

Base Information

Chemical Name:(3aS,4R,6S,6aR)-6-hydroxy-2,2-dimethyltetrahydro-3aH-cyclo-penta[d][1,3]dioxol-4-aminium (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate dibenzoyl-L-tartrate
CAS No.:1154413-15-6
Molecular Formula:C₈H₁₅NO₃*C₁₈H₁₄O₈
Molecular Weight:531.516
Hs Code.:

(3aS,4R,6S,6aR)-6-hydroxy-2,2-dimethyltetrahydro-3aH-cyclo-penta[d][1,3]dioxol-4-aminium (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate dibenzoyl-L-tartrate

Synonyms:(3aS,4R,6S,6aR)-6-hydroxy-2,2-dimethyltetrahydro-3aH-cyclo-penta[d][1,3]dioxol-4-aminium (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate dibenzoyl-L-tartrate

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Chemical Property of (3aS,4R,6S,6aR)-6-hydroxy-2,2-dimethyltetrahydro-3aH-cyclo-penta[d][1,3]dioxol-4-aminium (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate dibenzoyl-L-tartrate

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Technology Process of (3aS,4R,6S,6aR)-6-hydroxy-2,2-dimethyltetrahydro-3aH-cyclo-penta[d][1,3]dioxol-4-aminium (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate dibenzoyl-L-tartrate

There total 2 articles about (3aS,4R,6S,6aR)-6-hydroxy-2,2-dimethyltetrahydro-3aH-cyclo-penta[d][1,3]dioxol-4-aminium (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate dibenzoyl-L-tartrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 88756-83-6
(+/-)-1β-amino-2α,3α-O-isopropylidene-2α,3α,4β-cyclopentanetriol

: 2743-38-6
O,O'-dibenzoyl-L-tartaric acid

: 1154413-15-6
(3aS,4R,6S,6aR)-6-hydroxy-2,2-dimethyltetrahydro-3aH-cyclo-penta[d][1,3]dioxol-4-aminium (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate dibenzoyl-L-tartrate

Guidance literature:: In ethanol; water; at 20 - 70 ℃; for 2.1667 - 18h; Product distribution / selectivity;

Reference yield: 36.0%

: 2743-38-6
O,O'-dibenzoyl-L-tartaric acid

: (1S,2R,6R,7R)-4,4-Dimethyl-3,5,8-trioxa-9-aza-tricyclo[5.2.1.0^2,6]decane-9-carboxylic acid benzyl ester

: 1154413-15-6
(3aS,4R,6S,6aR)-6-hydroxy-2,2-dimethyltetrahydro-3aH-cyclo-penta[d][1,3]dioxol-4-aminium (2R,3R)-2,3-bis(benzoyloxy)-3-carboxypropanoate dibenzoyl-L-tartrate

Guidance literature:: (1S,2R,6R,7R)-4,4-Dimethyl-3,5,8-trioxa-9-aza-tricyclo[5.2.1.0^2,6]decane-9-carboxylic acid benzyl ester; With hydrogen; 5%-palladium/activated carbon; In ethanol; water; at 50 ℃; for 18h; under 6000.6 Torr;

O,O'-dibenzoyl-L-tartaric acid; In ethanol; water; at 18 - 28 ℃; for 4h; Product distribution / selectivity;