(S)-prolinol amide of allyl-3-cyclohexylpropionic acid

Base Information

Chemical Name:(S)-prolinol amide of allyl-3-cyclohexylpropionic acid
CAS No.:143668-92-2
Molecular Formula:C₁₇H₂₉NO₂
Molecular Weight:279.423
Hs Code.:

Synonyms:(S)-prolinol amide of allyl-3-cyclohexylpropionic acid

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Chemical Property of (S)-prolinol amide of allyl-3-cyclohexylpropionic acid

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Technology Process of (S)-prolinol amide of allyl-3-cyclohexylpropionic acid

There total 4 articles about (S)-prolinol amide of allyl-3-cyclohexylpropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1124-63-6
3-cyclohexylpropan-1-ol

: 143668-92-2
(S)-prolinol amide of allyl-3-cyclohexylpropionic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / Jones reagent / acetone / Ambient temperature

2: oxalyl chloride / 2 h / Heating

3: N-methylmorpholine / tetrahydrofuran / a) 0 deg C, 1 h, b) RT, overnight

4: 1.) LDA, 2.) tetrabutylammonium iodide / 1.) THF, 0 deg C, 2 h, 2.) THF, reflux, overnight

With 4-methyl-morpholine; jones reagent; oxalyl dichloride; tetra-(n-butyl)ammonium iodide; lithium diisopropyl amide; In tetrahydrofuran; acetone;
DOI:10.1021/ja00046a010

Reference yield:

: 701-97-3
cyclohexanepropionic acid

: 143668-92-2
(S)-prolinol amide of allyl-3-cyclohexylpropionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride / 2 h / Heating

2: N-methylmorpholine / tetrahydrofuran / a) 0 deg C, 1 h, b) RT, overnight

3: 1.) LDA, 2.) tetrabutylammonium iodide / 1.) THF, 0 deg C, 2 h, 2.) THF, reflux, overnight

With 4-methyl-morpholine; oxalyl dichloride; tetra-(n-butyl)ammonium iodide; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ja00046a010

Reference yield:

: 39098-75-4
3-cyclohexylpropionyl chloride

: 143668-92-2
(S)-prolinol amide of allyl-3-cyclohexylpropionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / tetrahydrofuran / a) 0 deg C, 1 h, b) RT, overnight

2: 1.) LDA, 2.) tetrabutylammonium iodide / 1.) THF, 0 deg C, 2 h, 2.) THF, reflux, overnight

With 4-methyl-morpholine; tetra-(n-butyl)ammonium iodide; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ja00046a010