2-(4-{[1-amino-3-(2,4-difluorophenyl)-3-oxoprop-1-en-1-yl]amino}-3,5-difluoro-phenyl)ethyl acetate

Base Information

Chemical Name:2-(4-{[1-amino-3-(2,4-difluorophenyl)-3-oxoprop-1-en-1-yl]amino}-3,5-difluoro-phenyl)ethyl acetate
CAS No.:1151805-62-7
Molecular Formula:C₁₉H₁₆F₄N₂O₃
Molecular Weight:396.341
Hs Code.:

Synonyms:2-(4-{[1-amino-3-(2,4-difluorophenyl)-3-oxoprop-1-en-1-yl]amino}-3,5-difluoro-phenyl)ethyl acetate

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Chemical Property of 2-(4-{[1-amino-3-(2,4-difluorophenyl)-3-oxoprop-1-en-1-yl]amino}-3,5-difluoro-phenyl)ethyl acetate

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Technology Process of 2-(4-{[1-amino-3-(2,4-difluorophenyl)-3-oxoprop-1-en-1-yl]amino}-3,5-difluoro-phenyl)ethyl acetate

There total 2 articles about 2-(4-{[1-amino-3-(2,4-difluorophenyl)-3-oxoprop-1-en-1-yl]amino}-3,5-difluoro-phenyl)ethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 602309-42-2
4-chlorophenyl 3-(2,4-difluorophenyl)-3-oxopropanimidothioate hydrochloride

: 1151805-51-4
2-(3,5-difluoro-4-nitrophenyl)ethanol

: 1151805-62-7
2-(4-{[1-amino-3-(2,4-difluorophenyl)-3-oxoprop-1-en-1-yl]amino}-3,5-difluoro-phenyl)ethyl acetate

Guidance literature:: 4-chlorophenyl 3-(2,4-difluorophenyl)-3-oxopropanimidothioate hydrochloride; 2-(3,5-difluoro-4-nitrophenyl)ethanol; In acetic acid; at 80 ℃; for 20h;

With sodium hydrogencarbonate; In water; ethyl acetate;

Reference yield: 67.0%

: 1151805-32-1
2-(4-amino-3,5-difluorophenyl)ethanol

: 1151805-61-6
3-amino-3-[(4-chlorophenyl)thio]-1-(2,4-difluorophenyl)prop-2-en-1-one hydrochloride

: 64-19-7,77671-22-8
acetic acid

: 1151805-62-7
2-(4-{[1-amino-3-(2,4-difluorophenyl)-3-oxoprop-1-en-1-yl]amino}-3,5-difluoro-phenyl)ethyl acetate

Guidance literature:: 2-(4-amino-3,5-difluorophenyl)ethanol; 3-amino-3-[(4-chlorophenyl)thio]-1-(2,4-difluorophenyl)prop-2-en-1-one hydrochloride; acetic acid; at 80 ℃; for 20h;

With sodium hydrogencarbonate; In water; ethyl acetate;

Reference yield: 37.0%

: 1151805-62-7
2-(4-{[1-amino-3-(2,4-difluorophenyl)-3-oxoprop-1-en-1-yl]amino}-3,5-difluoro-phenyl)ethyl acetate

: 471-25-0
Propiolic acid

: 1151805-63-8
2-{4-[6-amino-5-(2,4-difluorobenzoyl)-2-oxopyridin-1(2H)-yl]-3,5-difluorophenyl}ethyl acetate

Guidance literature:: Propiolic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 0 - 20 ℃; for 1.5h;

2-(4-{[1-amino-3-(2,4-difluorophenyl)-3-oxoprop-1-en-1-yl]amino}-3,5-difluoro-phenyl)ethyl acetate; In tetrahydrofuran; at 80 ℃; for 5h;