(6S,12S,15S,24S,30S,33S)-6,12,24,30-Tetrabenzyl-1,4,7,10,13,19,22,25,28,31-decaaza-tricyclo[31.3.0.0^15,19]hexatriacontane-2,5,8,11,14,20,23,26,29,32-decaone

Base Information

• Chemical Name: (6S,12S,15S,24S,30S,33S)-6,12,24,30-Tetrabenzyl-1,4,7,10,13,19,22,25,28,31-decaaza-tricyclo[31.3.0.0^15,19]hexatriacontane-2,5,8,11,14,20,23,26,29,32-decaone
• CAS No.: 82247-64-1
• Molecular Formula: C₅₄H₆₂N₁₀O₁₀
• Molecular Weight: 1011.15

Synonyms:(6S,12S,15S,24S,30S,33S)-6,12,24,30-Tetrabenzyl-1,4,7,10,13,19,22,25,28,31-decaaza-tricyclo[31.3.0.0^15,19]hexatriacontane-2,5,8,11,14,20,23,26,29,32-decaone

Chemical Property of (6S,12S,15S,24S,30S,33S)-6,12,24,30-Tetrabenzyl-1,4,7,10,13,19,22,25,28,31-decaaza-tricyclo[31.3.0.0^15,19]hexatriacontane-2,5,8,11,14,20,23,26,29,32-decaone

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Technology Process of (6S,12S,15S,24S,30S,33S)-6,12,24,30-Tetrabenzyl-1,4,7,10,13,19,22,25,28,31-decaaza-tricyclo[31.3.0.0^15,19]hexatriacontane-2,5,8,11,14,20,23,26,29,32-decaone

There total 4 articles about (6S,12S,15S,24S,30S,33S)-6,12,24,30-Tetrabenzyl-1,4,7,10,13,19,22,25,28,31-decaaza-tricyclo[31.3.0.0^15,19]hexatriacontane-2,5,8,11,14,20,23,26,29,32-decaone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

C54H66N12O10*2ClH (82247-69-6) → (6S,12S,15S,24S,30S,33S)-6,12,24,30-Tetrabenzyl-1,4,7,10,13,19,22,25,28,31-decaaza-tricyclo[31.3.0.015,19]hexatriacontane-2,5,8,11,14,20,23,26,29,32-decaone (82247-64-1)

Guidance literature:

With sodium nitrite; In water; N,N-dimethyl-formamide; at -15 ℃; for 0.5h;

DOI:10.1021/ja00381a006

Reference yield: 7.6%

(S)-Pyrrolidine-2-carboxylic acid [(S)-1-({[(S)-1-(hydrazinocarbonylmethyl-carbamoyl)-2-phenyl-ethylcarbamoyl]-methyl}-carbamoyl)-2-phenyl-ethyl]-amide; hydrochloride (82247-65-2) → 8,14-dibenzyl-dodecahydro-3a,6,9,12,15-pentaaza-cyclopentacyclopentadecene-4,7,10,13,16-pentaone (61898-89-3) + (6S,12S,15S,24S,30S,33S)-6,12,24,30-Tetrabenzyl-1,4,7,10,13,19,22,25,28,31-decaaza-tricyclo[31.3.0.015,19]hexatriacontane-2,5,8,11,14,20,23,26,29,32-decaone (82247-64-1)

Guidance literature:

With sodium nitrite; In water; N,N-dimethyl-formamide; at -15 ℃; for 0.5h;

DOI:10.1021/ja00381a006

Reference yield:

C60H74N10O13 (82247-67-4) → (6S,12S,15S,24S,30S,33S)-6,12,24,30-Tetrabenzyl-1,4,7,10,13,19,22,25,28,31-decaaza-tricyclo[31.3.0.015,19]hexatriacontane-2,5,8,11,14,20,23,26,29,32-decaone (82247-64-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 74 percent / hydrazine monohydrate / methanol / 2 h / 40 °C

2: 96 percent / 2N HCl / dioxane / 2 h

3: 37 percent / NaNO₂ / dimethylformamide; H₂O / 0.5 h / -15 °C

With hydrogenchloride; hydrazine hydrate; sodium nitrite; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;

DOI:10.1021/ja00381a006

upstream raw materials:

C₅₄H₆₆N₁₂O₁₀*2ClH

(S)-Pyrrolidine-2-carboxylic acid [(S)-1-({[(S)-1-(hydrazinocarbonylmethyl-carbamoyl)-2-phenyl-ethylcarbamoyl]-methyl}-carbamoyl)-2-phenyl-ethyl]-amide; hydrochloride

C₆₀H₇₄N₁₀O₁₃

C₅₉H₇₄N₁₂O₁₂

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