C₆₃H₅₆O₁₅

Base Information

• Chemical Name: C₆₃H₅₆O₁₅
• CAS No.: 1161867-80-6
• Molecular Formula: C₆₃H₅₆O₁₅
• Molecular Weight: 1053.13
• Mol file: 1161867-80-6.mol

Synonyms:C₆₃H₅₆O₁₅

Chemical Property of C₆₃H₅₆O₁₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₃H₅₆O₁₅

There total 6 articles about C₆₃H₅₆O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

{3-[3-benzyloxy-5-(3,5-bis-hydroxymethyl-phenoxymethyl)-benzyloxy]-5-hydroxymethyl-phenyl}-methanol (894094-41-8) + methyl 3-hydroxybenzoate (19438-10-9) → C63H56O15 (1161867-80-6)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; Inert atmosphere;

Reference yield:

benzyl alcohol (100-51-6,185532-71-2) → C63H56O15 (1161867-80-6)

Guidance literature:

Multi-step reaction with 5 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 12.17 h / 0 - 50 °C / Inert atmosphere; Schlenk technique

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Reflux; Inert atmosphere

3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 12.17 h / 0 - 50 °C / Inert atmosphere; Schlenk technique

4: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Reflux; Inert atmosphere; Schlenk technique

5: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 12.17 h / 0 - 50 °C / Inert atmosphere; Schlenk technique

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; 1: |Mitsunobu Displacement / 3: |Mitsunobu Displacement / 5: |Mitsunobu Displacement;

DOI:10.1002/chem.201400157

Reference yield:

[5-(benzyloxy)-1,3-phenylene]dimethanol (251912-48-8) → C63H56O15 (1161867-80-6)

Guidance literature:

Multi-step reaction with 3 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 12.17 h / 0 - 50 °C / Inert atmosphere; Schlenk technique

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Reflux; Inert atmosphere; Schlenk technique

3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 12.17 h / 0 - 50 °C / Inert atmosphere; Schlenk technique

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; 1: |Mitsunobu Displacement / 3: |Mitsunobu Displacement;

DOI:10.1002/chem.201400157

upstream raw materials:

{3-[3-benzyloxy-5-(3,5-bis-hydroxymethyl-phenoxymethyl)-benzyloxy]-5-hydroxymethyl-phenyl}-methanol

methyl 3-hydroxybenzoate

benzyl alcohol

dimethyl 5-(benzyloxy)isophthalate