1-[(2-benzothienylcarbonyl)amino]cyclohexanecarboxylic acid phenylmethyl ester

Base Information

Chemical Name:1-[(2-benzothienylcarbonyl)amino]cyclohexanecarboxylic acid phenylmethyl ester
CAS No.:944282-05-7
Molecular Formula:C₂₃H₂₃NO₃S
Molecular Weight:393.507
Hs Code.:

Synonyms:1-[(2-benzothienylcarbonyl)amino]cyclohexanecarboxylic acid phenylmethyl ester

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Chemical Property of 1-[(2-benzothienylcarbonyl)amino]cyclohexanecarboxylic acid phenylmethyl ester

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Technology Process of 1-[(2-benzothienylcarbonyl)amino]cyclohexanecarboxylic acid phenylmethyl ester

There total 1 articles about 1-[(2-benzothienylcarbonyl)amino]cyclohexanecarboxylic acid phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 6314-28-9
benzo[b]thiophene-2-carboxylic acid

: 102373-23-9
1-aminocyclohexanecarboxylic acid benzyl ester

: 944282-05-7
1-[(2-benzothienylcarbonyl)amino]cyclohexanecarboxylic acid phenylmethyl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃;

Reference yield: 80.0%

: 944282-05-7
1-[(2-benzothienylcarbonyl)amino]cyclohexanecarboxylic acid phenylmethyl ester

: 652171-96-5
1-(benzo[b]thiophene-2-carboxamido)cyclohexanecarboxylic acid

Guidance literature:: 1-[(2-benzothienylcarbonyl)amino]cyclohexanecarboxylic acid phenylmethyl ester; With sodium hydroxide; water; In tetrahydrofuran; for 72h; Heating / reflux;

With hydrogenchloride; In water;

Reference yield:

: 944282-05-7
1-[(2-benzothienylcarbonyl)amino]cyclohexanecarboxylic acid phenylmethyl ester

: 944282-38-6
N-[[1-[(2-benzothienylcarbonyl)amino]cyclohexyl]carbonyl]-L-phenylglycine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; water / tetrahydrofuran / 72 h / Heating / reflux

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / toluene / Heating / reflux

With sodium hydroxide; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; toluene;