imidazole-1-carbothioic acid O-(5-(1,2-bisbenzyloxyethyl)-2-methoxytetrahydrofuran-3-yl) ester

Base Information

Chemical Name:imidazole-1-carbothioic acid O-(5-(1,2-bisbenzyloxyethyl)-2-methoxytetrahydrofuran-3-yl) ester
CAS No.:1067648-38-7
Molecular Formula:C₂₅H₂₈N₂O₅S
Molecular Weight:468.574
Hs Code.:

Synonyms:imidazole-1-carbothioic acid O-(5-(1,2-bisbenzyloxyethyl)-2-methoxytetrahydrofuran-3-yl) ester

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Chemical Property of imidazole-1-carbothioic acid O-(5-(1,2-bisbenzyloxyethyl)-2-methoxytetrahydrofuran-3-yl) ester

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Technology Process of imidazole-1-carbothioic acid O-(5-(1,2-bisbenzyloxyethyl)-2-methoxytetrahydrofuran-3-yl) ester

There total 1 articles about imidazole-1-carbothioic acid O-(5-(1,2-bisbenzyloxyethyl)-2-methoxytetrahydrofuran-3-yl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1079398-63-2
methyl 5,6-di-O-benzyl-3-deoxy-D-glucofuranoside

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 1067648-38-7
imidazole-1-carbothioic acid O-(5-(1,2-bisbenzyloxyethyl)-2-methoxytetrahydrofuran-3-yl) ester

Guidance literature:: In tetrahydrofuran; Heating / reflux;

Reference yield:

: 1067648-38-7
imidazole-1-carbothioic acid O-(5-(1,2-bisbenzyloxyethyl)-2-methoxytetrahydrofuran-3-yl) ester

: 1067648-48-9
(2R,4S,5S)-5-azido-6-(3,5-difluorobenzyloxy)-4-hydroxy-2-methylhexanoic acid cyclopropylamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: tri-n-butyl-tin hydride / toluene / 2.5 h / 110 °C / Heating / reflux

2.1: boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 6 h / 0 - 20 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

3.2: 2 h / -78 °C

3.3: 20 °C

4.1: hydrogen / palladium on activated charcoal / ethanol

5.1: di(n-butyl)tin oxide / toluene / 5 h / Heating / reflux

5.2: 90 °C

6.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.17 h / -15 °C

6.2: 0 - 20 °C

7.1: trimethylaluminum / dichloromethane / 0.25 h

7.2: 1 h / 40 °C

With di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; hydrogen; trimethylaluminum; tri-n-butyl-tin hydride; di(n-butyl)tin oxide; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; toluene;

Reference yield:

: 1067648-38-7
imidazole-1-carbothioic acid O-(5-(1,2-bisbenzyloxyethyl)-2-methoxytetrahydrofuran-3-yl) ester

: 1067648-42-3
2,3-dideoxy-6-O-(3,5-difluorobenzyl)-2-methyl-D-glucono-1,4-lactone

Guidance literature:: Multi-step reaction with 5 steps

1.1: tri-n-butyl-tin hydride / toluene / 2.5 h / 110 °C / Heating / reflux

2.1: boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 6 h / 0 - 20 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

3.2: 2 h / -78 °C

3.3: 20 °C

4.1: hydrogen / palladium on activated charcoal / ethanol

5.1: di(n-butyl)tin oxide / toluene / 5 h / Heating / reflux

5.2: 90 °C

With boron trifluoride diethyl etherate; hydrogen; tri-n-butyl-tin hydride; di(n-butyl)tin oxide; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; toluene;