N'-(2-hydroxy-4-methoxybenzylidene)-3-methoxybenzohydrazide

Base Information

• Chemical Name: N'-(2-hydroxy-4-methoxybenzylidene)-3-methoxybenzohydrazide
• CAS No.: 677313-81-4
• Molecular Formula: C₁₆H₁₆N₂O₄
• Molecular Weight: 300.314
• Mol file: 677313-81-4.mol

Synonyms:N'-(2-hydroxy-4-methoxybenzylidene)-3-methoxybenzohydrazide

Chemical Property of N'-(2-hydroxy-4-methoxybenzylidene)-3-methoxybenzohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-(2-hydroxy-4-methoxybenzylidene)-3-methoxybenzohydrazide

There total 1 articles about N'-(2-hydroxy-4-methoxybenzylidene)-3-methoxybenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

2-Hydroxy-4-methoxybenzaldehyde (673-22-3) + 3-methoxybenzoic hydrazide (5785-06-8) → N'-(2-hydroxy-4-methoxybenzylidene)-3-methoxybenzohydrazide (677313-81-4)

Guidance literature:

In methanol; for 3h; Reflux;

DOI:10.1016/j.poly.2019.04.045

Reference yield: 61.0%

methanol (67-56-1) + bis(acetylacetonate)oxovanadium (3153-26-2) + N'-(2-hydroxy-4-methoxybenzylidene)-3-methoxybenzohydrazide (677313-81-4) → C34H34N4O12V2

Guidance literature:

at 20 ℃; for 0.5h;

DOI:10.1080/15533174.2012.680125

Reference yield: 32.0%

bis(acetylacetonato)dioxidomolybdenum(VI) + N'-(2-hydroxy-4-methoxybenzylidene)-3-methoxybenzohydrazide (677313-81-4) + dimethyl sulfoxide (67-68-5,8070-53-9) → (4-methoxysalicylaldehyde-3-methoxy-benzylhydrazonato)dimethylsulfoxidedioxidomolybdenum(VI)

Guidance literature:

In methanol; for 4h; Reflux;

DOI:10.1016/j.poly.2019.04.045

upstream raw materials:

2-Hydroxy-4-methoxybenzaldehyde

3-methoxybenzoic hydrazide