N,N-diethyl-N'-(4-methoxy-2-nitro-phenyl)-propanediyldiamine

Base Information

• Chemical Name: N,N-diethyl-N'-(4-methoxy-2-nitro-phenyl)-propanediyldiamine
• CAS No.: 854651-63-1
• Molecular Formula: C₁₄H₂₃N₃O₃
• Molecular Weight: 281.355
• Mol file: 854651-63-1.mol

Synonyms:N,N-diethyl-N'-(4-methoxy-2-nitro-phenyl)-propanediyldiamine

Chemical Property of N,N-diethyl-N'-(4-methoxy-2-nitro-phenyl)-propanediyldiamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-diethyl-N'-(4-methoxy-2-nitro-phenyl)-propanediyldiamine

There total 5 articles about N,N-diethyl-N'-(4-methoxy-2-nitro-phenyl)-propanediyldiamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-5-methoxynitrobenzene (10298-80-3) + diethylaminopropylamine (104-78-9) → N,N-diethyl-N'-(4-methoxy-2-nitro-phenyl)-propanediyldiamine (854651-63-1)

Guidance literature:

at 140 ℃;

DOI:10.1021/ja01215a037

Reference yield:

toluene-4-sulfonic acid-[N-(3-diethylamino-propyl)-4-methoxy-2-nitro-anilide] (674815-15-7) → N,N-diethyl-N'-(4-methoxy-2-nitro-phenyl)-propanediyldiamine (854651-63-1)

Guidance literature:

With sulfuric acid; at 0 ℃;

DOI:10.1039/jr9460000681

Reference yield:

N-(4-methoxy-2-nitrophenyl)-4-methylbenzenesulfonamide (3360-81-4) → N,N-diethyl-N'-(4-methoxy-2-nitro-phenyl)-propanediyldiamine (854651-63-1)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanolic sodium ethylate

2: sulfuric acid / 0 °C

With sulfuric acid; sodium ethanolate;

DOI:10.1039/jr9460000681

upstream raw materials:

toluene-4-sulfonic acid-[N-(3-diethylamino-propyl)-4-methoxy-2-nitro-anilide]

2-chloro-5-methoxynitrobenzene

diethylaminopropylamine

N-(4-methoxy-2-nitrophenyl)-4-methylbenzenesulfonamide

Downstream raw materials:

N¹-(3-diethylamino-propyl)-4-methoxy-o-phenylenediamine