N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide trifluoroacetate

Base Information

Chemical Name:N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide trifluoroacetate
CAS No.:1607465-05-3
Molecular Formula:C₂HF₃O₂*C₁₃H₁₄N₄O₂S
Molecular Weight:404.37
Hs Code.:

Synonyms:N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide trifluoroacetate

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Chemical Property of N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide trifluoroacetate

Chemical Property:

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Technology Process of N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide trifluoroacetate

There total 1 articles about N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134812-30-9
N-(4-(3'-aminophenyl)thiazol-2-yl)acetamide

: 1607465-05-3
N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 3 h / Reflux

2: dichloromethane / 24 h / 20 °C

With 2-chloro-1-methyl-pyridinium iodide; triethylamine; In dichloromethane;
DOI:10.1002/chem.201303664

Reference yield: 67.0%

: 1607465-05-3
N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide trifluoroacetate

: 20866-46-0
N,1'-bis[(1,1-dimethylethoxy)carbonyl]-L-histidine

: 1607465-10-0
Nα,Nδ-di-tert-butoxycarbonyl[N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide

Guidance literature:: With dmap; benzotriazol-1-ol; triethylamine; diisopropyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/chem.201303664

Reference yield:

: 1607465-05-3
N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide trifluoroacetate

: 1607465-13-3
[N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; benzotriazol-1-ol; diisopropyl-carbodiimide; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

With dmap; benzotriazol-1-ol; triethylamine; trifluoroacetic acid; diisopropyl-carbodiimide; In dichloromethane;
DOI:10.1002/chem.201303664