[N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide

Base Information

Chemical Name:[N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide
CAS No.:1607465-13-3
Molecular Formula:C₁₉H₂₁N₇O₃S
Molecular Weight:427.487
Hs Code.:

Synonyms:[N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide

Chemical Property:

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Technology Process of [N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide

There total 4 articles about [N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1607465-10-0
Nα,Nδ-di-tert-butoxycarbonyl[N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide

: 1607465-13-3
[N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1002/chem.201303664

Reference yield:

: 1607465-01-9
N-tert-butoxycarbonyl[N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)]-2-aminoacetamide

: 1607465-13-3
[N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 24 h / 20 °C

2: triethylamine; benzotriazol-1-ol; diisopropyl-carbodiimide; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

With dmap; benzotriazol-1-ol; triethylamine; trifluoroacetic acid; diisopropyl-carbodiimide; In dichloromethane;
DOI:10.1002/chem.201303664

Reference yield:

: 1607465-05-3
N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide trifluoroacetate

: 1607465-13-3
[N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-2-aminoacetamide]histidinamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; benzotriazol-1-ol; diisopropyl-carbodiimide; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

With dmap; benzotriazol-1-ol; triethylamine; trifluoroacetic acid; diisopropyl-carbodiimide; In dichloromethane;
DOI:10.1002/chem.201303664