Technology Process of C25H25F5N4O5S
There total 7 articles about C25H25F5N4O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
caesium carbonate;
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; DavePhos;
In
1,4-dioxane;
at 100 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; ammonium hydroxide / N,N-dimethyl-formamide / 4 h / 20 °C
2.1: borane-THF / tetrahydrofuran / 4 h / Reflux
3.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 2 h / 20 °C
4.1: Oxone / methanol / 2 h / 20 °C
4.2: 2 h / 20 °C
5.1: caesium carbonate / DavePhos; tris(dibenzylideneacetone)dipalladium(0) chloroform complex / 1,4-dioxane / 4 h / 100 °C
With
Oxone; ammonium hydroxide; borane-THF; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU;
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; DavePhos;
In
tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: water; lithium hydroxide / methanol / 4 h / 20 °C
2.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 2 h / 20 °C
3.1: Oxone / methanol / 2 h / 20 °C
3.2: 2 h / 20 °C
4.1: caesium carbonate / DavePhos; tris(dibenzylideneacetone)dipalladium(0) chloroform complex / 1,4-dioxane / 4 h / 100 °C
With
Oxone; water; caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide;
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; DavePhos;
In
1,4-dioxane; methanol; N,N-dimethyl-formamide;