S-phenyl 4'-hydroxythiobenzoate

Base Information

Chemical Name:S-phenyl 4'-hydroxythiobenzoate
CAS No.:81787-28-2
Molecular Formula:C₁₃H₁₀O₂S
Molecular Weight:230.287
Hs Code.:

Synonyms:S-phenyl 4'-hydroxythiobenzoate

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Chemical Property of S-phenyl 4'-hydroxythiobenzoate

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Technology Process of S-phenyl 4'-hydroxythiobenzoate

There total 5 articles about S-phenyl 4'-hydroxythiobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 108-98-5
thiophenol

: 99-96-7
4-hydroxy-benzoic acid

: 81787-28-2
S-phenyl 4'-hydroxythiobenzoate

Guidance literature:: With PPE; for 15h; Ambient temperature;
DOI:10.1055/s-1982-29716

Reference yield: 80.0%

: 106-41-2
4-bromo-phenol

: 108-98-5
thiophenol

: 82102-37-2
9-methyl-9H-fluorene-9-carbonyl chloride

: 81787-28-2
S-phenyl 4'-hydroxythiobenzoate

Guidance literature:: 4-bromo-phenol; thiophenol; With bis(benzonitrile)palladium(II) dichloride; sodium acetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium iodide; Inert atmosphere; Glovebox;

9-methyl-9H-fluorene-9-carbonyl chloride; With N-Methyldicyclohexylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; at 120 ℃; for 24h; Inert atmosphere; Glovebox;
DOI:10.1021/jo5009965

Reference yield: 41.0%

: 5351-23-5
4-hydroxybenzoic acid hydrazide

: 882-33-7
diphenyldisulfane

: 81787-28-2
S-phenyl 4'-hydroxythiobenzoate

Guidance literature:: With ammonium peroxydisulfate; copper(l) cyanide; In dimethyl sulfoxide; at 100 ℃; for 6h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.0c02328