(3-chlorophenyl)phenylmethyl methyl ether

Base Information

• Chemical Name: (3-chlorophenyl)phenylmethyl methyl ether
• CAS No.: 27401-83-8
• Molecular Formula: C₁₄H₁₃ClO
• Molecular Weight: 232.71
• Mol file: 27401-83-8.mol

Synonyms:(3-chlorophenyl)phenylmethyl methyl ether

Chemical Property of (3-chlorophenyl)phenylmethyl methyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (3-chlorophenyl)phenylmethyl methyl ether

There total 4 articles about (3-chlorophenyl)phenylmethyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3-iodochlorobenzene (625-99-0) + benzaldehyde dimethyl acetal (1125-88-8) → (3-chlorophenyl)phenylmethyl methyl ether (27401-83-8)

Guidance literature:

With chloro-trimethyl-silane; [nickel(II)dichloride(dimethoxyethane)]; N,N-dimethyl acetamide; 2,6-bis(pyrazole)pyridine; zinc; at 23 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1002/anie.201503936

Reference yield: 6.0%

triphenyl(3-chlorophenyl)methane (115228-81-4) → biphenyl (92-52-4,1594-86-1) + m-chlorobiphenyl (2051-61-8) + benzhydryl methyl ether (1016-09-7) + (3-chlorophenyl)phenylmethyl methyl ether (27401-83-8)

Guidance literature:

In methanol; benzene; for 4h; Product distribution; Quantum yield; Irradiation;

DOI:10.1246/bcsj.63.2731

Reference yield:

methanol (67-56-1) + 3-chlorobenzhydryl chloride (13391-39-4) → (3-chlorophenyl)phenylmethyl methyl ether (27401-83-8)

Guidance literature:

With potassium chloride; at 35 ℃; Rate constant; also with CH₃OD;

DOI:10.1021/jo00129a016

upstream raw materials:

triphenyl(3-chlorophenyl)methane

methanol

(3-chlorophenyl)phenylbromomethane

3-chlorobenzhydryl chloride