11-amino-3-(4-hydroxyphenyl)-3H-5,10,12,12a-tetraazabenzo[4,5]cycloocta[1,2,3-cd]inden-4(5H)-one

Base Information

Chemical Name:11-amino-3-(4-hydroxyphenyl)-3H-5,10,12,12a-tetraazabenzo[4,5]cycloocta[1,2,3-cd]inden-4(5H)-one
CAS No.:1426668-44-1
Molecular Formula:C₂₀H₁₇N₅O₃
Molecular Weight:375.387
Hs Code.:

Synonyms:11-amino-3-(4-hydroxyphenyl)-3H-5,10,12,12a-tetraazabenzo[4,5]cycloocta[1,2,3-cd]inden-4(5H)-one

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Chemical Property of 11-amino-3-(4-hydroxyphenyl)-3H-5,10,12,12a-tetraazabenzo[4,5]cycloocta[1,2,3-cd]inden-4(5H)-one

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Technology Process of 11-amino-3-(4-hydroxyphenyl)-3H-5,10,12,12a-tetraazabenzo[4,5]cycloocta[1,2,3-cd]inden-4(5H)-one

There total 11 articles about 11-amino-3-(4-hydroxyphenyl)-3H-5,10,12,12a-tetraazabenzo[4,5]cycloocta[1,2,3-cd]inden-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1426668-49-6
methyl 2-(4-(2-aminophenyl)-2-(methoxycarbonylamino)pyrrolo[1,2-f][1,2,4]triazin-5-yl)-2-(4-hydroxyphenyl)acetate

: 1426668-44-1
11-amino-3-(4-hydroxyphenyl)-3H-5,10,12,12a-tetraazabenzo[4,5]cycloocta[1,2,3-cd]inden-4(5H)-one

Guidance literature:: With water; sodium hydroxide; In methanol; for 5h; Reflux;

Reference yield:

: 1426668-46-3
methyl 3-(4-hydroxyphenyl)-10-((methoxycarbonyl)amino)-3,4-dihydro-4,9,11,11a-tetraazadibenzo[cd,f]azulene-3-carboxylate

: 1426668-44-1
11-amino-3-(4-hydroxyphenyl)-3H-5,10,12,12a-tetraazabenzo[4,5]cycloocta[1,2,3-cd]inden-4(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol; water / 82 h / 2844.39 Torr

2: water; sodium hydroxide / methanol / 5 h / Reflux

With hydrogenchloride; palladium 10% on activated carbon; water; hydrogen; sodium hydroxide; In methanol; water;

Reference yield:

: 1426663-88-8
methyl (4-(2-aminophenyl)pyrrolo[2,1-f][1,2,4]triazin-2-yl)carbamate

: 1426668-44-1
11-amino-3-(4-hydroxyphenyl)-3H-5,10,12,12a-tetraazabenzo[4,5]cycloocta[1,2,3-cd]inden-4(5H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / 1,4-dioxane; methanol / 48 h / 100 °C / Sealed tube

2: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol; water / 82 h / 2844.39 Torr

3: water; sodium hydroxide / methanol / 5 h / Reflux

With hydrogenchloride; palladium 10% on activated carbon; water; hydrogen; sodium hydroxide; In 1,4-dioxane; methanol; water;