Technology Process of C29H29N5O5
There total 6 articles about C29H29N5O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
at 50 ℃;
for 3h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C
1.2: 2 h / 0 °C
2.1: water; sodium hydroxide / tetrahydrofuran / -10 - 20 °C
3.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / acetonitrile / 0 - 20 °C
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C
5.1: 3 h / 50 °C / Inert atmosphere
With
water; sodium hydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; acetonitrile; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / acetonitrile / 0 - 20 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C
3: 3 h / 50 °C / Inert atmosphere
With
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; acetonitrile;