5-{2-methyl-2-[(2-phenylethyl)carbamoyl]ethyl}furan-2-carboxylic acid 4-amidinophenyl ester trifluoroacetic acid salt

Base Information

Chemical Name:5-{2-methyl-2-[(2-phenylethyl)carbamoyl]ethyl}furan-2-carboxylic acid 4-amidinophenyl ester trifluoroacetic acid salt
CAS No.:1311288-52-4
Molecular Formula:C₂HF₃O₂*C₂₄H₂₅N₃O₄
Molecular Weight:533.504
Hs Code.:

Synonyms:5-{2-methyl-2-[(2-phenylethyl)carbamoyl]ethyl}furan-2-carboxylic acid 4-amidinophenyl ester trifluoroacetic acid salt

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Chemical Property of 5-{2-methyl-2-[(2-phenylethyl)carbamoyl]ethyl}furan-2-carboxylic acid 4-amidinophenyl ester trifluoroacetic acid salt

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Technology Process of 5-{2-methyl-2-[(2-phenylethyl)carbamoyl]ethyl}furan-2-carboxylic acid 4-amidinophenyl ester trifluoroacetic acid salt

There total 7 articles about 5-{2-methyl-2-[(2-phenylethyl)carbamoyl]ethyl}furan-2-carboxylic acid 4-amidinophenyl ester trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1311287-69-0
3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropionic acid trifluoroacetic acid salt

: 64-04-0
phenethylamine

: 1311288-52-4
5-{2-methyl-2-[(2-phenylethyl)carbamoyl]ethyl}furan-2-carboxylic acid 4-amidinophenyl ester trifluoroacetic acid salt

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In pyridine; at 20 ℃; for 2h;

Reference yield:

: 13529-17-4
5-Formyl-2-furancarboxylic acid

: 1311288-52-4
5-{2-methyl-2-[(2-phenylethyl)carbamoyl]ethyl}furan-2-carboxylic acid 4-amidinophenyl ester trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 7 steps

1.1: hexane; acetone / 0.17 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

2.2: 0 - 20 °C

3.1: lithium hydroxide / water; methanol / 1.67 h / 20 °C

3.2: 0.17 h

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / pyridine / 20 °C

5.1: 0.25 h / 20 °C

6.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / pyridine / 2 h / 20 °C

With hydrogen; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; pyridine; methanol; hexane; water; acetone;

Reference yield:

: 5904-71-2
methyl 5-formylfuran-2-carboxylate

: 1311288-52-4
5-{2-methyl-2-[(2-phenylethyl)carbamoyl]ethyl}furan-2-carboxylic acid 4-amidinophenyl ester trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

1.2: 0 - 20 °C

2.1: lithium hydroxide / water; methanol / 1.67 h / 20 °C

2.2: 0.17 h

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / pyridine / 20 °C

4.1: 0.25 h / 20 °C

5.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / pyridine / 2 h / 20 °C

With hydrogen; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; pyridine; methanol; water;