Technology Process of C11H7ClO4S
There total 4 articles about C11H7ClO4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron tribromide;
In
dichloromethane;
at -78 - 20 ℃;
for 10h;
Inert atmosphere;
DOI:10.1016/j.bmcl.2013.02.019
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / dimethyl sulfoxide / 10 h / 80 °C / Inert atmosphere
2: sodium chlorite; potassium dihydrogenphosphate / tetrahydrofuran; dimethyl sulfoxide; tert-butyl alcohol; water / 48 h / 20 °C
3: boron tribromide / dichloromethane / 10 h / -78 - 20 °C / Inert atmosphere
With
sodium chlorite; potassium dihydrogenphosphate; boron tribromide; potassium carbonate;
In
tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.02.019
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium chlorite; potassium dihydrogenphosphate / tetrahydrofuran; dimethyl sulfoxide; tert-butyl alcohol; water / 48 h / 20 °C
2: boron tribromide / dichloromethane / 10 h / -78 - 20 °C / Inert atmosphere
With
sodium chlorite; potassium dihydrogenphosphate; boron tribromide;
In
tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.02.019