1-Benzyl-2,4-dimethyl-3-carbomethoxy-6-carbethoxy-7-oxopyrrolo<3,2-b>pyridine

Base Information

Chemical Name:1-Benzyl-2,4-dimethyl-3-carbomethoxy-6-carbethoxy-7-oxopyrrolo<3,2-b>pyridine
CAS No.:97653-34-4
Molecular Formula:C₂₁H₂₂N₂O₅
Molecular Weight:382.416
Hs Code.:

Synonyms:1-Benzyl-2,4-dimethyl-3-carbomethoxy-6-carbethoxy-7-oxopyrrolo<3,2-b>pyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Benzyl-2,4-dimethyl-3-carbomethoxy-6-carbethoxy-7-oxopyrrolo<3,2-b>pyridine

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Technology Process of 1-Benzyl-2,4-dimethyl-3-carbomethoxy-6-carbethoxy-7-oxopyrrolo<3,2-b>pyridine

There total 6 articles about 1-Benzyl-2,4-dimethyl-3-carbomethoxy-6-carbethoxy-7-oxopyrrolo<3,2-b>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 97653-31-1
2-{[(1-Benzyl-4-methoxycarbonyl-5-methyl-1H-pyrrol-3-yl)-methyl-amino]-methylene}-malonic acid diethyl ester

: 97653-34-4
1-Benzyl-2,4-dimethyl-3-carbomethoxy-6-carbethoxy-7-oxopyrrolo<3,2-b>pyridine

Guidance literature:: With polyphosphoric ester; at 95 - 100 ℃; for 2.5h;
DOI:10.1002/jhet.5570220122

Reference yield:

: 100-39-0
benzyl bromide

: 97653-34-4
1-Benzyl-2,4-dimethyl-3-carbomethoxy-6-carbethoxy-7-oxopyrrolo<3,2-b>pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / sodium methoxide / dimethylformamide / 1 h / Ambient temperature

2: 87 percent / Dowtherm A / 0.5 h / Heating

3: sodium methoxide / dimethylformamide / Ambient temperature; overnight

With diphenyl ether-biphenyl eutectic; sodium methylate; In N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570220122

Reference yield:

: 97653-29-7
N-<2-Methyl-3-carbomethoxypyrrol-4-yl>aminomethylenemalonic Acid, Diethyl Ester

: 97653-34-4
1-Benzyl-2,4-dimethyl-3-carbomethoxy-6-carbethoxy-7-oxopyrrolo<3,2-b>pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / sodium methoxide / dimethylformamide / 1 h / Ambient temperature

2: 87 percent / Dowtherm A / 0.5 h / Heating

3: sodium methoxide / dimethylformamide / Ambient temperature; overnight

With diphenyl ether-biphenyl eutectic; sodium methylate; In N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570220122