1-bromo-5,7-dimethyl-6-(4-methylphenyl)-2-phenyl-2,6-dihydro-1H-pyrrolo[3,4-d][1,2,3]diazaphosphinine

Base Information

• Chemical Name: 1-bromo-5,7-dimethyl-6-(4-methylphenyl)-2-phenyl-2,6-dihydro-1H-pyrrolo[3,4-d][1,2,3]diazaphosphinine
• CAS No.: 400770-40-3
• Molecular Formula: C₂₀H₁₉BrN₃P
• Molecular Weight: 412.269

Synonyms:1-bromo-5,7-dimethyl-6-(4-methylphenyl)-2-phenyl-2,6-dihydro-1H-pyrrolo[3,4-d][1,2,3]diazaphosphinine

Chemical Property of 1-bromo-5,7-dimethyl-6-(4-methylphenyl)-2-phenyl-2,6-dihydro-1H-pyrrolo[3,4-d][1,2,3]diazaphosphinine

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Technology Process of 1-bromo-5,7-dimethyl-6-(4-methylphenyl)-2-phenyl-2,6-dihydro-1H-pyrrolo[3,4-d][1,2,3]diazaphosphinine

There total 1 articles about 1-bromo-5,7-dimethyl-6-(4-methylphenyl)-2-phenyl-2,6-dihydro-1H-pyrrolo[3,4-d][1,2,3]diazaphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

N-(2,5-dimethyl-1-p-tolyl-1H-pyrrol-3-ylmethylene)-N'-phenyl-hydrazine → 1-bromo-5,7-dimethyl-6-(4-methylphenyl)-2-phenyl-2,6-dihydro-1H-pyrrolo[3,4-d][1,2,3]diazaphosphinine (400770-40-3)

Guidance literature:

With phosphorus tribromide; In pyridine; for 24h;

DOI:10.1002/hc.1099

Reference yield: 72.0%

morpholine (110-91-8,99108-56-2) + phenylhydrazine (100-63-0) + 1-bromo-5,7-dimethyl-6-(4-methylphenyl)-2-phenyl-2,6-dihydro-1H-pyrrolo[3,4-d][1,2,3]diazaphosphinine (400770-40-3) → N-[5,7-dimethyl-6-(4-methylphenyl)-1-(4-morpholinyl)-2-phenyl-2,6-dihydro-1H-1λ5-pyrrolo[3,4-d][1,2,3]diazaphosphinin-1-ylidene]aniline

Guidance literature:

morpholine; 1-bromo-5,7-dimethyl-6-(4-methylphenyl)-2-phenyl-2,6-dihydro-1H-pyrrolo[3,4-d][1,2,3]diazaphosphinine; With triethylamine; In benzene; for 2h;

phenylhydrazine; In benzene; at 60 ℃; for 1h;

DOI:10.1002/hc.1099

Reference yield: 55.0%

morpholine (110-91-8,99108-56-2) + 1-bromo-5,7-dimethyl-6-(4-methylphenyl)-2-phenyl-2,6-dihydro-1H-pyrrolo[3,4-d][1,2,3]diazaphosphinine (400770-40-3) → 5,7-dimethyl-6-(4-methylphenyl)-1-(4-morpholinyl)-2-phenyl-2,6-dihydro-1H-1λ5-pyrrolo[3,4-d][1,2,3]diazaphosphinine-1-thione

Guidance literature:

morpholine; 1-bromo-5,7-dimethyl-6-(4-methylphenyl)-2-phenyl-2,6-dihydro-1H-pyrrolo[3,4-d][1,2,3]diazaphosphinine; With triethylamine; In benzene; for 2h;

With sulfur; In benzene; for 1h; Heating;

DOI:10.1002/hc.1099

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