N₁-((1R,1'R,3R,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine

Base Information

• Chemical Name: N₁-((1R,1'R,3R,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine
• CAS No.: 1126795-15-0
• Molecular Formula: C₂₃H₃₅N₃
• Molecular Weight: 353.551

Synonyms:N₁-((1R,1'R,3R,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine

Chemical Property of N₁-((1R,1'R,3R,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine

Chemical Property:

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Technology Process of N₁-((1R,1'R,3R,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine

There total 7 articles about N₁-((1R,1'R,3R,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(1R,1'R,3R,3'R,5S,5'S)-N-(2-nitrophenyl)-9'-aza[3,9'-bi(bicyclo[3.3.1]nonan)]-3'-amine (1126795-21-8) → N1-((1R,1'R,3R,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine (1126795-15-0)

Guidance literature:

(1R,1'R,3R,3'R,5S,5'S)-N-(2-nitrophenyl)-9'-aza[3,9'-bi(bicyclo[3.3.1]nonan)]-3'-amine; With hydrogen; palladium 10% on activated carbon; In methanol; at 25 ℃; for 1.5h;

With ammonia; In water; Product distribution / selectivity;

Reference yield: 78.8%

(1R,1'R,3r,5S,5'S)-9'-aza[3,9′-bi(bicyclo[3.3.1]nonan)]-3'-one + 1,2-diamino-benzene (95-54-5) → N1-((1R,1'R,3R,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine (1126795-15-0)

Guidance literature:

(1R,1'R,3r,5S,5'S)-9'-aza[3,9′-bi(bicyclo[3.3.1]nonan)]-3'-one; 1,2-diamino-benzene; With acetic acid; In 1,2-dimethoxyethane; at 25 ℃; for 16h; Inert atmosphere;

With sodium tris(acetoxy)borohydride; In 1,2-dimethoxyethane; at 25 ℃; for 6h;

With sodium hydroxide; In methanol; water; at 40 ℃; pH=8 - 9; Product distribution / selectivity;

Reference yield: 59.0%

9-((exo)-bicyclo[3.3.1]nonan-3-yl)-9-azabicyclo[3.3.1]nonan-3-one (1126795-13-8) + 1,2-diamino-benzene (95-54-5) → N1-((1R,1'R,3R,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine (1126795-15-0)

Guidance literature:

With sodium tetrahydroborate; 2-Ethylhexanoic acid; In dichloromethane; at 0 - 60 ℃; for 16.75h; Product distribution / selectivity;

upstream raw materials:

9-((exo)-bicyclo[3.3.1]nonan-3-yl)-9-azabicyclo[3.3.1]nonan-3-one

1,2-diamino-benzene

(1R,1'R,3R,3'R,5S,5'S)-N-(2-nitrophenyl)-9'-aza[3,9'-bi(bicyclo[3.3.1]nonan)]-3'-amine

(1R,1'R,3R,3'R,5S,5'S)-9'-aza[3,9'-bi(bicyclo[3.3.1]nonan)]-3'-amine acetate

Downstream raw materials:

ethyl 2-(3-(2-((1R,1'R,3r,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-ylamino)phenyl)ureido)acetate

2-((2-((1R,1'R,3r,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-ylamino)phenyl)amino)-2-oxoethyl acetate

2-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyclo[3.3.1]nonan)]-3'-yl(2-(carboxyformamido)phenyl)amino)-2-oxoacetic acid

N₁-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyco[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine

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