4-{[1-Chloro-1-phenyl-meth-(Z)-ylidene]-amino}-benzoic acid ethyl ester

Base Information

Chemical Name:4-{[1-Chloro-1-phenyl-meth-(Z)-ylidene]-amino}-benzoic acid ethyl ester
CAS No.:52807-34-8
Molecular Formula:C₁₆H₁₄ClNO₂
Molecular Weight:287.746
Hs Code.:

Synonyms:4-{[1-Chloro-1-phenyl-meth-(Z)-ylidene]-amino}-benzoic acid ethyl ester

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Chemical Property of 4-{[1-Chloro-1-phenyl-meth-(Z)-ylidene]-amino}-benzoic acid ethyl ester

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Technology Process of 4-{[1-Chloro-1-phenyl-meth-(Z)-ylidene]-amino}-benzoic acid ethyl ester

There total 2 articles about 4-{[1-Chloro-1-phenyl-meth-(Z)-ylidene]-amino}-benzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 736-40-3
N-benzoylbenzocaine

: 52807-34-8
4-{[1-Chloro-1-phenyl-meth-(Z)-ylidene]-amino}-benzoic acid ethyl ester

Guidance literature:: With phosphorus pentachloride; In dichloromethane; at 20 ℃; for 1h; Schlenk technique;
DOI:10.1039/c4dt00372a

Reference yield:

: 98-88-4
benzoyl chloride

: 94-09-7
p-aminoethylbenzoate

: 52807-34-8
4-{[1-Chloro-1-phenyl-meth-(Z)-ylidene]-amino}-benzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 20 °C / Schlenk technique

2: phosphorus pentachloride / dichloromethane / 1 h / 20 °C / Schlenk technique

With phosphorus pentachloride; In dichloromethane;
DOI:10.1039/c4dt00372a

Reference yield: 84.0%

: 52807-34-8
4-{[1-Chloro-1-phenyl-meth-(Z)-ylidene]-amino}-benzoic acid ethyl ester

: 7182-99-2
4-benzylidenamino-benzoic acid ethyl ester

Guidance literature:: With hydrogen; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In benzene; at 120 ℃; for 4h; under 36775.4 Torr;
DOI:10.1055/s-1985-31406