cis-4-<<3-(4-chlorophenyl)-2-methyl-3-<(1H-1,2,4-triazol-1-yl)methyl>isoxazolidin-5-yl>methoxy>benzoic acid

Base Information

• Chemical Name: cis-4-<<3-(4-chlorophenyl)-2-methyl-3-<(1H-1,2,4-triazol-1-yl)methyl>isoxazolidin-5-yl>methoxy>benzoic acid
• CAS No.: 124172-25-4
• Molecular Formula: C₂₁H₂₁ClN₄O₄
• Molecular Weight: 428.875

Synonyms:cis-4-<<3-(4-chlorophenyl)-2-methyl-3-<(1H-1,2,4-triazol-1-yl)methyl>isoxazolidin-5-yl>methoxy>benzoic acid

Chemical Property of cis-4-<<3-(4-chlorophenyl)-2-methyl-3-<(1H-1,2,4-triazol-1-yl)methyl>isoxazolidin-5-yl>methoxy>benzoic acid

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Technology Process of cis-4-<<3-(4-chlorophenyl)-2-methyl-3-<(1H-1,2,4-triazol-1-yl)methyl>isoxazolidin-5-yl>methoxy>benzoic acid

There total 3 articles about cis-4-<<3-(4-chlorophenyl)-2-methyl-3-<(1H-1,2,4-triazol-1-yl)methyl>isoxazolidin-5-yl>methoxy>benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

methyl cis-4-<<3-(4-chlorophenyl)-2-methyl-3-<(1H-1,2,4-triazol-1-yl)methyl>isoxazolidin-5-yl>methoxy>benzoate (114544-58-0,114544-70-6,114544-71-7) → cis-4-<<3-(4-chlorophenyl)-2-methyl-3-<(1H-1,2,4-triazol-1-yl)methyl>isoxazolidin-5-yl>methoxy>benzoic acid (124172-25-4)

Guidance literature:

With potassium hydroxide; In ethanol; for 1.5h; Heating;

DOI:10.1002/jhet.5570260639

Reference yield:

1-(4-chlorophenyl)-N-methyl-2-(1H-1,2,4-triazol-1-yl)-ethanimine N-oxide (119393-53-2,121263-17-0,114371-22-1) → cis-4-<<3-(4-chlorophenyl)-2-methyl-3-<(1H-1,2,4-triazol-1-yl)methyl>isoxazolidin-5-yl>methoxy>benzoic acid (124172-25-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 29 percent / toluene / 48 h / Heating

2: 68 percent / potassium hydroxide / aq. ethanol / 1.5 h / Heating

With potassium hydroxide; In ethanol; toluene;

DOI:10.1002/jhet.5570260639

Reference yield:

methyl 4-allyloxybenzoate (35750-24-4) → cis-4-<<3-(4-chlorophenyl)-2-methyl-3-<(1H-1,2,4-triazol-1-yl)methyl>isoxazolidin-5-yl>methoxy>benzoic acid (124172-25-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 29 percent / toluene / 48 h / Heating

2: 68 percent / potassium hydroxide / aq. ethanol / 1.5 h / Heating

With potassium hydroxide; In ethanol; toluene;

DOI:10.1002/jhet.5570260639

upstream raw materials:

methyl cis-4-<<3-(4-chlorophenyl)-2-methyl-3-<(1H-1,2,4-triazol-1-yl)methyl>isoxazolidin-5-yl>methoxy>benzoate

methyl 4-allyloxybenzoate

1-(4-chlorophenyl)-N-methyl-2-(1H-1,2,4-triazol-1-yl)-ethanimine N-oxide

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