(4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride

Base Information

Chemical Name:(4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride
CAS No.:850568-55-7
Molecular Formula:C13H20 B N O2 . Cl H
Molecular Weight:269.579
Hs Code.:2931900090
European Community (EC) Number:692-575-5
DSSTox Substance ID:DTXSID00930136
Mol file:850568-55-7.mol

Synonyms:850568-55-7;(4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride;4-Aminomethylphenylboronic acid, pinacol ester, HCl;4-Aminomethylphenylboronic acid pinacol ester hydrochloride;4-Aminomethylphenylboronic acid pinacol ester HCl;[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine hydrochloride;4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)benzylamine hydrochloride;1-[4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYL]METHANAMINE HYDROCHLORIDE;KPECMJIHZZWTJN-UHFFFAOYSA-N;[4-(tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine hydrochloride;DTXSID00930136;AMY32951;Benzenemethanamine,4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-;MFCD02179455;AKOS015911422;AB11166;AS-2563;(4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYL)METHANAMINE HCL;[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine;hydrochloride;CS-0174692;EN300-1698805;A807396;A863741;J-514434;Z3217366816;4-Aminomethylohenylboronic acid pinacl ester hydrochloride;4-Aminomethylphenylboronic acid, pinacol ester hydrochloride;4-(Aminomethyl)benzeneboronic acid, pinacol ester hydrochloride;4-(Aminomethyl)phenylboronic acid pinacol ester hydrochloride, 97%;4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzylamine hydrochloride;(4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanaminehydrochloride;1-[4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine--hydrogen chloride (1/1)

Suppliers and Price of (4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-(Aminomethyl)phenylboronic acid pinacol ester hydrochloride
1g
$ 175.00

Synthonix
4-(Aminomethyl)phenylboronic acid pinacol ester hydrochloride 96%
25g
$ 2025.00

SynQuest Laboratories
4-(Aminomethyl)benzeneboronic acid, pinacol ester hydrochloride
1 g
$ 192.00

SynQuest Laboratories
4-(Aminomethyl)benzeneboronic acid, pinacol ester hydrochloride
250 mg
$ 64.00

Sigma-Aldrich
4-(Aminomethyl)phenylboronic acid pinacol ester hydrochloride 97%
500mg
$ 83.30

Sigma-Aldrich
4-(Aminomethyl)phenylboronic acid pinacol ester hydrochloride 97%
1g
$ 124.00

Crysdot
(4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanaminehydrochloride 95+%
1g
$ 95.00

Crysdot
(4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanaminehydrochloride 95+%
5g
$ 310.00

American Custom Chemicals Corporation
4-AMINO METHYL PHENYL BORONIC ACID, PINACOL ESTER HYDROCHLORIDE 95.00%
1G
$ 349.65

Alichem
(4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanaminehydrochloride
5g
$ 278.72

Total 24 raw suppliers

Chemical Property of (4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride

Chemical Property:

Melting Point:228-238℃
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:269.1353868
Heavy Atom Count:18
Complexity:257

Purity/Quality:

97% ^*data from raw suppliers

4-(Aminomethyl)phenylboronic acid pinacol ester hydrochloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)C2=CC=C(C=C2)CN.Cl
Uses 4-Aminomethylphenylboronic acid, pinacol ester, HCl

Technology Process of (4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride

There total 2 articles about (4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 68819-84-1
tert-butyl N-(4-bromobenzyl)carbamate

: 73183-34-3
bis(pinacol)diborane

: 850568-55-7
(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 100 ℃; for 12h;
DOI:10.1016/j.tetlet.2012.11.001

Reference yield:

: 128376-64-7
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde

: 850568-55-7
(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride

Guidance literature:: 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde; With ammonia; hydrogen; In tert-butyl alcohol; at 120 ℃; for 24h; Autoclave; High pressure;

With hydrogenchloride; at 20 ℃;
DOI:10.1002/anie.201812100

Reference yield: 95.0%

: 75-44-5
phosgene

: 850568-55-7
(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride

: 2-(4-(isocyanatomethyl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: (4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanamine hydrochloride; With triethylamine; In 1,4-dioxane; for 0.5h;

phosgene; at 21 ℃; for 16h; Inert atmosphere;