tert-butyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Base Information

Chemical Name:tert-butyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate
CAS No.:1205536-99-7
Molecular Formula:C₃₁H₄₇NO₃Si
Molecular Weight:509.805
Hs Code.:

Synonyms:tert-butyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Suppliers and Price of tert-butyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

There total 7 articles about tert-butyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1205536-97-5
(1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutan-1-amine

: 1205536-99-7
tert-butyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 1205536-95-3
benzyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

: 1205536-99-7
tert-butyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate; methanol / 8 h / 20 °C / 760.05 Torr / Inert atmosphere

2: triethylamine / dichloromethane / 28 h / 0 - 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; dichloromethane; ethyl acetate;

Reference yield:

: 1205536-82-8
(S,E)-8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-amine hydrochloride

: 1205536-99-7
tert-butyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C

2.1: diethylzinc / dichloromethane; 1,2-dimethoxyethane / 0.23 h / -20 - 20 °C / Inert atmosphere

2.2: 10 h / 20 °C

3.1: palladium 10% on activated carbon; hydrogen / ethyl acetate; methanol / 8 h / 20 °C / 760.05 Torr / Inert atmosphere

4.1: triethylamine / dichloromethane / 28 h / 0 - 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; diethylzinc; triethylamine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; ethyl acetate;