(1S,5S,7R)-N-methyl-2β-phenyl-3-p-tolyl-7β-(p-tolylthio)-8-azabicyclo<3.2.1>oct-3-ene

Base Information

• Chemical Name: (1S,5S,7R)-N-methyl-2β-phenyl-3-p-tolyl-7β-(p-tolylthio)-8-azabicyclo<3.2.1>oct-3-ene
• CAS No.: 208989-38-2
• Molecular Formula: C₂₈H₂₉NS
• Molecular Weight: 411.611

Synonyms:(1S,5S,7R)-N-methyl-2β-phenyl-3-p-tolyl-7β-(p-tolylthio)-8-azabicyclo<3.2.1>oct-3-ene

Chemical Property of (1S,5S,7R)-N-methyl-2β-phenyl-3-p-tolyl-7β-(p-tolylthio)-8-azabicyclo<3.2.1>oct-3-ene

Chemical Property:

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Technology Process of (1S,5S,7R)-N-methyl-2β-phenyl-3-p-tolyl-7β-(p-tolylthio)-8-azabicyclo<3.2.1>oct-3-ene

There total 2 articles about (1S,5S,7R)-N-methyl-2β-phenyl-3-p-tolyl-7β-(p-tolylthio)-8-azabicyclo<3.2.1>oct-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylmagnesium bromide (100-58-3) + (1S,5S,6R)-2-acetoxy-N-methyl-3-p-tolyl-6β-(p-tolylthio)-8-azabicyclo<3.2.1>oct-3-ene → (1S,5S,7R)-N-methyl-2β-phenyl-3-p-tolyl-7β-(p-tolylthio)-8-azabicyclo<3.2.1>oct-3-ene (208989-38-2)

Guidance literature:

With 1.) CuCN; Yield given; Multistep reaction; 1.) Et₂O, -7 deg C, 10 min, 2.) Et₂O, RT, 1.5 h;

DOI:10.1021/jm9802564

Reference yield:

→ (1S,5S,7R)-N-methyl-2β-phenyl-3-p-tolyl-7β-(p-tolylthio)-8-azabicyclo<3.2.1>oct-3-ene (208989-38-2)

Guidance literature:

Reference yield: 50.0%

(1S,5S,7R)-N-methyl-2β-phenyl-3-p-tolyl-7β-(p-tolylthio)-8-azabicyclo<3.2.1>oct-3-ene (208989-38-2) → (1S,5S)-N-methyl-2β-phenyl-3β-p-tolyltropane (208989-27-9)

Guidance literature:

With Ra-Ni; In ethanol; for 2h; Heating;

DOI:10.1021/jm9802564

upstream raw materials:

phenylmagnesium bromide

Downstream raw materials:

(1S,5S)-N-methyl-2β-phenyl-3β-p-tolyltropane

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