Technology Process of C41H41N3O7S
There total 9 articles about C41H41N3O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap;
In
pyridine;
at 20 ℃;
for 72h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: lithium borohydride / tetrahydrofuran / 16 h / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
2.2: 12 h
3.1: carbon tetrabromide; triethylamine; sodium azide; triphenylphosphine / N,N-dimethyl-formamide / 25 h / Inert atmosphere
4.1: hydrogen / 5%-palladium/activated carbon / methanol / 5 h / 20 °C
5.1: chloroform-d1 / 5 h / Inert atmosphere; Reflux
6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
7.1: dmap / pyridine / 72 h / 20 °C
With
dmap; lithium borohydride; sodium azide; carbon tetrabromide; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; triethylamine; triphenylphosphine;
5%-palladium/activated carbon;
In
tetrahydrofuran; pyridine; methanol; chloroform-d1; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: carbon tetrabromide; triethylamine; sodium azide; triphenylphosphine / N,N-dimethyl-formamide / 25 h / Inert atmosphere
2: hydrogen / 5%-palladium/activated carbon / methanol / 5 h / 20 °C
3: chloroform-d1 / 5 h / Inert atmosphere; Reflux
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
5: dmap / pyridine / 72 h / 20 °C
With
dmap; sodium azide; carbon tetrabromide; tetrabutyl ammonium fluoride; hydrogen; triethylamine; triphenylphosphine;
5%-palladium/activated carbon;
In
tetrahydrofuran; pyridine; methanol; chloroform-d1; N,N-dimethyl-formamide;