Formaldehyde-13C, d2 solution

Base Information

• Chemical Name: Formaldehyde-13C, d2 solution
• CAS No.: 63101-50-8
• Molecular Formula: CH₂O
• Molecular Weight: 32.9994

Synonyms:paraformaldehyde-¹³C-d₂

Chemical Property of Formaldehyde-13C, d2 solution

Chemical Property:

• Flash Point: 113?°C

Purity/Quality:

≥99% atom 13C; ≥98% atom D ^*data from raw suppliers

Formaldehyde-13C,D2(20%inD2O) ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 20/21/22-36/37/38-40-43
• Safety Statements: 26-36/37-51

MSDS Files:

SDS file from LookChem

Useful:

• Uses: (Formaldehyde-13C, d2) Labelled Formaldehyde, used in various organic synthesis and reactions. It is used in the textile industry in the area of crosslinking molecules to vary the properties of fabrics. In the food industry it is used to reinforce and improve packaging of meats and produce. It can help improve the water resistance of biodegradable collagen films.

Technology Process of Formaldehyde-13C, d2 solution

There total 2 articles about Formaldehyde-13C, d2 solution which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[13C]Carbon monoxide (1641-69-6) → [13C,2H4]methyl alcohol (32479-98-4) + paraformaldehyde-13C-d2 (63101-50-8,43094-80-0,89277-65-6) + deuterio-[13C]formyl (75491-79-1) + carbon dioxide (1111-72-4) + (13)C(2)HO2 + (13)C(2)H2O2

Guidance literature:

With water; for 2h; Irradiation;

DOI:10.1002/anie.201901059

Reference yield:

C36(13)CH30(2)H2O2Si2 → paraformaldehyde-13C-d2 (63101-50-8,43094-80-0,89277-65-6)

Guidance literature:

With cesium fluoride; In acetonitrile; at 20 ℃; for 0.166667h;

DOI:10.1021/jacs.9b08342

Reference yield: 98.0%

paraformaldehyde-13C-d2 (63101-50-8,43094-80-0,89277-65-6) + 4-nitro-aniline (100-01-6,104810-17-5) → 4-nitro-N,N-bis(dideuteriomethyl-13C)aniline

Guidance literature:

With sodium tetrahydroborate; sulfuric acid; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/ja00118a001

upstream raw materials:

[13C]Carbon monoxide

Downstream raw materials:

C₇⁽¹³⁾CH₇⁽²⁾H₂ClO

[(13)CD3]-asenapine

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