(η-1,5-cyclooctadiene)(cyanomethane)(tricyclohexylphosphine)iridium(I) tetrafluoroborate

Base Information

Chemical Name:(η-1,5-cyclooctadiene)(cyanomethane)(tricyclohexylphosphine)iridium(I) tetrafluoroborate
CAS No.:80409-87-6
Molecular Formula:BF₄*C₂₈H₄₈IrNP
Molecular Weight:708.694
Hs Code.:

Synonyms:(η-1,5-cyclooctadiene)(cyanomethane)(tricyclohexylphosphine)iridium(I) tetrafluoroborate

Suppliers and Price of (η-1,5-cyclooctadiene)(cyanomethane)(tricyclohexylphosphine)iridium(I) tetrafluoroborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η-1,5-cyclooctadiene)(cyanomethane)(tricyclohexylphosphine)iridium(I) tetrafluoroborate

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Technology Process of (η-1,5-cyclooctadiene)(cyanomethane)(tricyclohexylphosphine)iridium(I) tetrafluoroborate

There total 1 articles about (η-1,5-cyclooctadiene)(cyanomethane)(tricyclohexylphosphine)iridium(I) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 14104-20-2
silver tetrafluoroborate

: 64536-83-0
IrClC₈H₁₂P(C₆H₁₁)3

: 75-05-8,26809-02-9
acetonitrile

: 80409-87-6
(η-1,5-cyclooctadiene)(cyanomethane)(tricyclohexylphosphine)iridium(I) tetrafluoroborate

Guidance literature:: In dichloromethane; byproducts: AgCl; The mixt. of reagents in CH2Cl2 was stirred at 25°C under N2 for30 min;; filtered, reduced in vac., treated with Et2O; elem. anal.;;

Reference yield: 76.0%

: 80409-87-6
(η-1,5-cyclooctadiene)(cyanomethane)(tricyclohexylphosphine)iridium(I) tetrafluoroborate

: 80409-85-4
(IrH₂(CH₃CN)P(C₆H₁₁)3)3H⁽²⁺⁾*2BF₄^(1-)

Guidance literature:: With H₂; In dichloromethane; byproducts: cyclooctene; A soln. of complex in CH2Cl2 was treated with H2 at 0°C for 15 min;; filtered, reduced in vol., pptd. with ether, recrystd. from CH2Cl2-Et2O; elem. anal.;;