(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzyl alcohol

Base Information

Chemical Name:(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzyl alcohol
CAS No.:114916-24-4
Molecular Formula:C₁₆H₁₉NO₅S₂
Molecular Weight:369.463
Hs Code.:

Synonyms:(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzyl alcohol

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Chemical Property of (+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzyl alcohol

Chemical Property:

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Technology Process of (+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzyl alcohol

There total 4 articles about (+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72856-73-6
2-methoxy-4-(methylsulfanyl)benzoic acid

: 114916-24-4
(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzyl alcohol

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / 2 h / Heating

2: 93 percent / triethylamine / toluene / Heating

3: 89 percent / tetrahydrofuran / 1 h / Heating

4: 23 percent / potassium permanganate / pyridine / 6 h / 50 - 60 °C

5: 50 percent / sodium hydroxide / methanol / 1 h / Heating

6: 52 percent / lithium aluminium hydride / tetrahydrofuran

With sodium hydroxide; potassium permanganate; lithium aluminium tetrahydride; thionyl chloride; triethylamine; In tetrahydrofuran; pyridine; methanol; toluene;
DOI:10.1016/S0040-4020(01)86895-2

Reference yield:

: 69883-78-9
2-methoxy-4-(methylthio)benzoyl chloride

: 114916-24-4
(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzyl alcohol

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / triethylamine / toluene / Heating

2: 89 percent / tetrahydrofuran / 1 h / Heating

3: 23 percent / potassium permanganate / pyridine / 6 h / 50 - 60 °C

4: 50 percent / sodium hydroxide / methanol / 1 h / Heating

5: 52 percent / lithium aluminium hydride / tetrahydrofuran

With sodium hydroxide; potassium permanganate; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; pyridine; methanol; toluene;
DOI:10.1016/S0040-4020(01)86895-2

Reference yield:

: 114916-79-9
2-methoxy-4-methylthiobenzoic acid menthyl ester

: 114916-24-4
(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzyl alcohol

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / tetrahydrofuran / 1 h / Heating

2: 23 percent / potassium permanganate / pyridine / 6 h / 50 - 60 °C

3: 50 percent / sodium hydroxide / methanol / 1 h / Heating

4: 52 percent / lithium aluminium hydride / tetrahydrofuran

With sodium hydroxide; potassium permanganate; lithium aluminium tetrahydride; In tetrahydrofuran; pyridine; methanol;
DOI:10.1016/S0040-4020(01)86895-2