LDN-209964

Base Information

Chemical Name:LDN-209964
CAS No.:1233355-53-7
Molecular Formula:C₁₉H₂₀N₂OS
Molecular Weight:324.447
Hs Code.:

Synonyms:LDN-209964

Suppliers and Price of LDN-209964

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of LDN-209964

Chemical Property:

Purity/Quality:

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Technology Process of LDN-209964

There total 6 articles about LDN-209964 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18617-96-4
2-Phenyl-4-merapto-6-methoxychinolin

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 1233355-53-7
LDN-209964

Guidance literature:: 2-Phenyl-4-merapto-6-methoxychinolin; 3-bromopropylamine tert-butylcarbamate; With potassium hydroxide; tetra-(n-butyl)ammonium iodide; In water; toluene; at 110 ℃;

With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃;

Reference yield:

: C₂₄H₂₈N₂O₃S

: 1233355-53-7
LDN-209964

Guidance literature:: With hydrogenchloride; methanol; In 1,4-dioxane; at 20 ℃;
DOI:10.1016/j.bmcl.2010.04.150

Reference yield:

: 6342-63-8
1-(2-bromo-5-methoxyphenyl)ethanone

: 1233355-53-7
LDN-209964

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; N,N`-dimethylethylenediamine / copper(l) iodide / toluene / 170 °C

2.1: sodium hydroxide / 1,4-dioxane / 110 °C

3.1: Lawessons reagent / tetrahydrofuran / 150 °C / Microwave irradiation

4.1: potassium hydroxide / tetra-(n-butyl)ammonium iodide / toluene; water / 110 °C

4.2: 20 °C

With Lawessons reagent; potassium carbonate; potassium hydroxide; sodium hydroxide; N,N`-dimethylethylenediamine; copper(l) iodide; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; 1,4-dioxane; water; toluene;