rac/meso-dichloridobis[1-propyl-1'-(2-methoxyphenyl)-η⁵-cyclopentadienyl]titanium

Base Information

• Chemical Name: rac/meso-dichloridobis[1-propyl-1'-(2-methoxyphenyl)-η⁵-cyclopentadienyl]titanium
• CAS No.: 1448675-69-1
• Molecular Formula: C₃₀H₃₄Cl₂O₂Ti
• Molecular Weight: 545.385

Synonyms:rac/meso-dichloridobis[1-propyl-1'-(2-methoxyphenyl)-η⁵-cyclopentadienyl]titanium

Chemical Property of rac/meso-dichloridobis[1-propyl-1'-(2-methoxyphenyl)-η⁵-cyclopentadienyl]titanium

Chemical Property:

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Technology Process of rac/meso-dichloridobis[1-propyl-1'-(2-methoxyphenyl)-η⁵-cyclopentadienyl]titanium

There total 1 articles about rac/meso-dichloridobis[1-propyl-1'-(2-methoxyphenyl)-η⁵-cyclopentadienyl]titanium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

1-[1-(cyclopenta-1,3-dien-1-yl)propyl]-2-methoxybenzene (1448675-82-8) + titanium tetrachloride (7550-45-0) → rac/meso-dichloridobis[1-propyl-1'-(2-methoxyphenyl)-η5-cyclopentadienyl]titanium (1448675-69-1)

Guidance literature:

1-[1-(cyclopenta-1,3-dien-1-yl)propyl]-2-methoxybenzene; With n-butyllithium; In diethyl ether; hexane; at 0 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

titanium tetrachloride; In tetrahydrofuran; toluene; at 20 - 85 ℃; for 16h; Schlenk technique; Inert atmosphere;

DOI:10.1002/anie.201508034

upstream raw materials:

1-[1-(cyclopenta-1,3-dien-1-yl)propyl]-2-methoxybenzene

titanium tetrachloride

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