4-bromo-3,5-bis((methylamino)methyl)benzene tert-butyldimethylsilyl ether

Base Information

Chemical Name:4-bromo-3,5-bis((methylamino)methyl)benzene tert-butyldimethylsilyl ether
CAS No.:410531-60-1
Molecular Formula:C₁₆H₂₉BrN₂OSi
Molecular Weight:373.409
Hs Code.:

Synonyms:4-bromo-3,5-bis((methylamino)methyl)benzene tert-butyldimethylsilyl ether

Suppliers and Price of 4-bromo-3,5-bis((methylamino)methyl)benzene tert-butyldimethylsilyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-bromo-3,5-bis((methylamino)methyl)benzene tert-butyldimethylsilyl ether

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-bromo-3,5-bis((methylamino)methyl)benzene tert-butyldimethylsilyl ether

There total 3 articles about 4-bromo-3,5-bis((methylamino)methyl)benzene tert-butyldimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 182629-25-0
5-{[(1,1-dimethylethyl)dimethylsilyl]oxy}benzene-1,3-dimethanol

: 410531-60-1
4-bromo-3,5-bis((methylamino)methyl)benzene tert-butyldimethylsilyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / PyH*Br₃; Fe / methanol; CH₂Cl₂ / 1 h / 20 °C

2: Et₃N / CH₂Cl₂ / 1.5 h / -78 °C

3: 0.95 g / CH₂Cl₂ / -78 - 20 °C

With iron; pyridinium hydrobromide perbromide; triethylamine; In methanol; dichloromethane;
DOI:10.1002/1521-3765(20020104)8:1<45::AID-CHEM45>3.0.CO;2-P

Reference yield:

: 410531-59-8
4-bromo-3,5-bis(hydroxymethyl)benzene tert-butyldimethylsilyl ether

: 410531-60-1
4-bromo-3,5-bis((methylamino)methyl)benzene tert-butyldimethylsilyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1.5 h / -78 °C

2: 0.95 g / CH₂Cl₂ / -78 - 20 °C

With triethylamine; In dichloromethane;
DOI:10.1002/1521-3765(20020104)8:1<45::AID-CHEM45>3.0.CO;2-P