5'-O-[benzhydryloxy-bis(trimethylsilyloxy)silyl]-N₆-(4,4'-dimethoxytrityl)-2'-deoxyadenosine

Base Information

• Chemical Name: 5'-O-[benzhydryloxy-bis(trimethylsilyloxy)silyl]-N₆-(4,4'-dimethoxytrityl)-2'-deoxyadenosine
• CAS No.: 904291-42-5
• Molecular Formula: C₅₀H₅₉N₅O₈Si₃
• Molecular Weight: 942.304

Synonyms:5'-O-[benzhydryloxy-bis(trimethylsilyloxy)silyl]-N₆-(4,4'-dimethoxytrityl)-2'-deoxyadenosine

Chemical Property of 5'-O-[benzhydryloxy-bis(trimethylsilyloxy)silyl]-N₆-(4,4'-dimethoxytrityl)-2'-deoxyadenosine

Chemical Property:

Purity/Quality:

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Technology Process of 5'-O-[benzhydryloxy-bis(trimethylsilyloxy)silyl]-N₆-(4,4'-dimethoxytrityl)-2'-deoxyadenosine

There total 2 articles about 5'-O-[benzhydryloxy-bis(trimethylsilyloxy)silyl]-N₆-(4,4'-dimethoxytrityl)-2'-deoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.9%

N6-dimethoxytrityl-2'-deoxyadenosine (130999-19-8) + benzhydryloxy-bis(trimethylsilyloxy)silyl chloride (309963-45-9) → 5'-O-[benzhydryloxy-bis(trimethylsilyloxy)silyl]-N6-(4,4'-dimethoxytrityl)-2'-deoxyadenosine (904291-42-5)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; Cooling with ice;

DOI:10.1080/10426500701734745

Reference yield: 67.9%

→ 5'-O-[benzhydryloxy-bis(trimethylsilyloxy)silyl]-N6-(4,4'-dimethoxytrityl)-2'-deoxyadenosine (904291-42-5)

Guidance literature:

Reference yield: 86.4%

5'-O-[benzhydryloxy-bis(trimethylsilyloxy)silyl]-N6-(4,4'-dimethoxytrityl)-2'-deoxyadenosine (904291-42-5) + bis(N,N-diisopropylamino)methoxyphosphine (92611-10-4) → C57H75N6O9PSi3 (904291-46-9)

Guidance literature:

With 1H-tetrazole; In dichloromethane; for 4h;

DOI:10.1080/10426500701734745

upstream raw materials:

N⁶-dimethoxytrityl-2'-deoxyadenosine

benzhydryloxy-bis(trimethylsilyloxy)silyl chloride

Downstream raw materials:

C₅₇H₇₅N₆O₉PSi₃

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