N-(3-(3-[(phenylsulfonyl)amino]phenyl)-1H-pyrazol-5-yl)-3-morpholinobenzamide

Base Information

Chemical Name:N-(3-(3-[(phenylsulfonyl)amino]phenyl)-1H-pyrazol-5-yl)-3-morpholinobenzamide
CAS No.:1327167-30-5
Molecular Formula:C₂₆H₂₅N₅O₄S
Molecular Weight:503.582
Hs Code.:

Synonyms:N-(3-(3-[(phenylsulfonyl)amino]phenyl)-1H-pyrazol-5-yl)-3-morpholinobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-(3-[(phenylsulfonyl)amino]phenyl)-1H-pyrazol-5-yl)-3-morpholinobenzamide

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Technology Process of N-(3-(3-[(phenylsulfonyl)amino]phenyl)-1H-pyrazol-5-yl)-3-morpholinobenzamide

There total 5 articles about N-(3-(3-[(phenylsulfonyl)amino]phenyl)-1H-pyrazol-5-yl)-3-morpholinobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₁N₅O₂

: 98-09-9
benzenesulfonyl chloride

: 1327167-30-5
N-(3-(3-[(phenylsulfonyl)amino]phenyl)-1H-pyrazol-5-yl)-3-morpholinobenzamide

Guidance literature:: With pyridine; In dimethyl sulfoxide; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2011.06.016

Reference yield:

: 221876-07-9
3-morpholinobenzoyl chloride

: 1327167-30-5
N-(3-(3-[(phenylsulfonyl)amino]phenyl)-1H-pyrazol-5-yl)-3-morpholinobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 1 h / 20 °C

2: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol; water / 12 h / 20 °C

3: pyridine / dimethyl sulfoxide / 1 h / 20 °C

With pyridine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; In methanol; water; dimethyl sulfoxide;
DOI:10.1016/j.bmc.2011.06.016

Reference yield:

: C₂₀H₁₉N₅O₄

: 1327167-30-5
N-(3-(3-[(phenylsulfonyl)amino]phenyl)-1H-pyrazol-5-yl)-3-morpholinobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol; water / 12 h / 20 °C

2: pyridine / dimethyl sulfoxide / 1 h / 20 °C

With pyridine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; In methanol; water; dimethyl sulfoxide;
DOI:10.1016/j.bmc.2011.06.016