p-nitrophenyl 2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

Base Information

Chemical Name:p-nitrophenyl 2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside
CAS No.:1316822-99-7
Molecular Formula:C₂₀H₂₀N₄O₈
Molecular Weight:444.401
Hs Code.:

Synonyms:p-nitrophenyl 2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-nitrophenyl 2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of p-nitrophenyl 2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

There total 4 articles about p-nitrophenyl 2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 210418-04-5
C₁₂H₁₄N₄O₇

: 1316822-99-7
p-nitrophenyl 2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃; for 1h;
DOI:10.1016/j.carres.2011.03.036

Reference yield:

: 1147438-51-4
p-nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside

: 1316822-99-7
p-nitrophenyl 2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 0.5 h / 20 °C / pH 10

1.2: Dowex H+

2.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide; acetonitrile / 1 h / 20 °C

With sodium methylate; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.carres.2011.03.036

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1316822-99-7
p-nitrophenyl 2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -20 °C

2.1: sodium methylate / methanol / 0.5 h / 20 °C / pH 10

2.2: Dowex H+

3.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide; acetonitrile / 1 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.carres.2011.03.036