3-methyl-5-(3-methyl-1-phenyl-1H-pyrazol-5-yloxy)-4-nitro-1-phenyl-1H-pyrazole

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Chemical Name:3-methyl-5-(3-methyl-1-phenyl-1H-pyrazol-5-yloxy)-4-nitro-1-phenyl-1H-pyrazole
CAS No.:1608125-54-7
Molecular Formula:C₂₀H₁₇N₅O₃
Molecular Weight:375.387
Hs Code.:

Synonyms:3-methyl-5-(3-methyl-1-phenyl-1H-pyrazol-5-yloxy)-4-nitro-1-phenyl-1H-pyrazole

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Chemical Property of 3-methyl-5-(3-methyl-1-phenyl-1H-pyrazol-5-yloxy)-4-nitro-1-phenyl-1H-pyrazole

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Technology Process of 3-methyl-5-(3-methyl-1-phenyl-1H-pyrazol-5-yloxy)-4-nitro-1-phenyl-1H-pyrazole

There total 3 articles about 3-methyl-5-(3-methyl-1-phenyl-1H-pyrazol-5-yloxy)-4-nitro-1-phenyl-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 89-25-8
edaravone

: 13551-76-3
5-chloro-3-methyl-4-nitro-1-phenyl-1H-pyrazole

: 1608125-54-7
3-methyl-5-(3-methyl-1-phenyl-1H-pyrazol-5-yloxy)-4-nitro-1-phenyl-1H-pyrazole

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 0.2h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.bmc.2014.03.016

Reference yield:

: 89-25-8
edaravone

: 1608125-54-7
3-methyl-5-(3-methyl-1-phenyl-1H-pyrazol-5-yloxy)-4-nitro-1-phenyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 2 h / Reflux

2: acetic anhydride; nitric acid / 4 h / 0 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 0.2 h / 80 °C / Inert atmosphere; Microwave irradiation

With nitric acid; acetic anhydride; potassium carbonate; trichlorophosphate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2014.03.016

Reference yield:

: 1131-17-5
5-chloro-3-methyl-1-phenyl-1H-pyrazole

: 1608125-54-7
3-methyl-5-(3-methyl-1-phenyl-1H-pyrazol-5-yloxy)-4-nitro-1-phenyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride; nitric acid / 4 h / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 0.2 h / 80 °C / Inert atmosphere; Microwave irradiation

With nitric acid; acetic anhydride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2014.03.016