2-Benzoyl-1-(2-carbethoxy-3-methoxybenzyl)-1-cyan-1,2-dihydroisochinolin

Base Information

Chemical Name:2-Benzoyl-1-(2-carbethoxy-3-methoxybenzyl)-1-cyan-1,2-dihydroisochinolin
CAS No.:145103-20-4
Molecular Formula:C₂₈H₂₄N₂O₄
Molecular Weight:452.51
Hs Code.:

Synonyms:2-Benzoyl-1-(2-carbethoxy-3-methoxybenzyl)-1-cyan-1,2-dihydroisochinolin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Benzoyl-1-(2-carbethoxy-3-methoxybenzyl)-1-cyan-1,2-dihydroisochinolin

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Technology Process of 2-Benzoyl-1-(2-carbethoxy-3-methoxybenzyl)-1-cyan-1,2-dihydroisochinolin

There total 2 articles about 2-Benzoyl-1-(2-carbethoxy-3-methoxybenzyl)-1-cyan-1,2-dihydroisochinolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 844-25-7,55839-33-3
2-benzoyl-1-cyano-1,2-dihydroisoquinoline

: 86823-81-6
6-bromomethyl-2-methoxy-benzoic acid ethyl ester

: 145103-20-4
2-Benzoyl-1-(2-carbethoxy-3-methoxybenzyl)-1-cyan-1,2-dihydroisochinolin

Guidance literature:: With sodium hydroxide; cetyltrimethylammonim bromide; In benzene; for 40h;
DOI:10.1007/BF00811549

Reference yield:

: 6520-83-8
ethyl 2-methoxy-6-methylbenzoate

: 145103-20-4
2-Benzoyl-1-(2-carbethoxy-3-methoxybenzyl)-1-cyan-1,2-dihydroisochinolin

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / N-bromosuccinimide (freshly prepared), benzoyl peroxide (wet) / CCl₄ / 10 h / Heating

2: 75 percent / cetrimonium bromide, 50percent aq. NaOH / benzene / 40 h

With sodium hydroxide; N-Bromosuccinimide; Perbenzoic acid; cetyltrimethylammonim bromide; In tetrachloromethane; benzene;
DOI:10.1007/BF00811549