(E)-N-((3-(phenylselanyl)propylcarbamoyl)methyl)-N-(4-methoxyphenyl)cinnamamide

Base Information

Chemical Name:(E)-N-((3-(phenylselanyl)propylcarbamoyl)methyl)-N-(4-methoxyphenyl)cinnamamide
CAS No.:1612261-03-6
Molecular Formula:C₂₇H₂₈N₂O₃Se
Molecular Weight:507.491
Hs Code.:

Synonyms:(E)-N-((3-(phenylselanyl)propylcarbamoyl)methyl)-N-(4-methoxyphenyl)cinnamamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-((3-(phenylselanyl)propylcarbamoyl)methyl)-N-(4-methoxyphenyl)cinnamamide

Chemical Property:

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Technology Process of (E)-N-((3-(phenylselanyl)propylcarbamoyl)methyl)-N-(4-methoxyphenyl)cinnamamide

There total 3 articles about (E)-N-((3-(phenylselanyl)propylcarbamoyl)methyl)-N-(4-methoxyphenyl)cinnamamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 140-10-3
(E)-3-phenylacrylic acid

: 1187664-48-7
(3-isocyanopropyl)(phenyl)selane

: 104-94-9
4-methoxy-aniline

: 1612261-03-6
(E)-N-((3-(phenylselanyl)propylcarbamoyl)methyl)-N-(4-methoxyphenyl)cinnamamide

Guidance literature:: In water; at 20 ℃;
DOI:10.1016/j.bmc.2014.05.019

Reference yield:

: C₁₀H₁₃NOSe

: 1612261-03-6
(E)-N-((3-(phenylselanyl)propylcarbamoyl)methyl)-N-(4-methoxyphenyl)cinnamamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisopropylamine; trichlorophosphate / dichloromethane / 0 °C

1.2: 25 - 35 °C

2.1: water / 20 °C

With diisopropylamine; trichlorophosphate; In dichloromethane; water; 2.1: |Ugi Condensation;
DOI:10.1016/j.bmc.2014.05.019

Reference yield:

: 125424-56-8
3-(phenylseleno)propylamine

: 1612261-03-6
(E)-N-((3-(phenylselanyl)propylcarbamoyl)methyl)-N-(4-methoxyphenyl)cinnamamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic anhydride / 2 h / Heating

2.1: diisopropylamine; trichlorophosphate / dichloromethane / 0 °C

2.2: 25 - 35 °C

3.1: water / 20 °C

With acetic anhydride; diisopropylamine; trichlorophosphate; In dichloromethane; water; 3.1: |Ugi Condensation;
DOI:10.1016/j.bmc.2014.05.019