3-(3-(tert-butoxyamino)-3-oxopropylamino)-N-(2,6-dibromo-4-(perfluoropropan-2-yl)phenyl)-2-fluorobenzamide

Base Information

Chemical Name:3-(3-(tert-butoxyamino)-3-oxopropylamino)-N-(2,6-dibromo-4-(perfluoropropan-2-yl)phenyl)-2-fluorobenzamide
CAS No.:1207315-09-0
Molecular Formula:C₂₃H₂₁Br₂F₈N₃O₃
Molecular Weight:699.233
Hs Code.:

Synonyms:3-(3-(tert-butoxyamino)-3-oxopropylamino)-N-(2,6-dibromo-4-(perfluoropropan-2-yl)phenyl)-2-fluorobenzamide

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Chemical Property of 3-(3-(tert-butoxyamino)-3-oxopropylamino)-N-(2,6-dibromo-4-(perfluoropropan-2-yl)phenyl)-2-fluorobenzamide

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Technology Process of 3-(3-(tert-butoxyamino)-3-oxopropylamino)-N-(2,6-dibromo-4-(perfluoropropan-2-yl)phenyl)-2-fluorobenzamide

There total 2 articles about 3-(3-(tert-butoxyamino)-3-oxopropylamino)-N-(2,6-dibromo-4-(perfluoropropan-2-yl)phenyl)-2-fluorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1207315-06-7
3-(3-(2,6-dibromo-4-(perfluoropropan-2-yl)phenylcarbamoyl)-2-fluorophenylamino)propanoic acid

: 39684-28-1
O-(tert-butyl)hydroxylamine hydrochloride

: 1207315-09-0
3-(3-(tert-butoxyamino)-3-oxopropylamino)-N-(2,6-dibromo-4-(perfluoropropan-2-yl)phenyl)-2-fluorobenzamide

Guidance literature:: 3-(3-(2,6-dibromo-4-(perfluoropropan-2-yl)phenylcarbamoyl)-2-fluorophenylamino)propanoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 0 ℃; for 1h;

O-(tert-butyl)hydroxylamine hydrochloride; With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

: 1207314-94-0
N-(2,6-dibromo-4-heptafluoroisopropylphenyl)-3-amino-2-fluorobenzamide

: 1207315-09-0
3-(3-(tert-butoxyamino)-3-oxopropylamino)-N-(2,6-dibromo-4-(perfluoropropan-2-yl)phenyl)-2-fluorobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3 h / 60 - 80 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 1 h / 0 °C

2.2: 0 - 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran;