1-[2-(3,3,5,5-tetramethylcyclohexyl)phenyl]piperazine methanesulfonic acid salt

Base Information

Chemical Name:1-[2-(3,3,5,5-tetramethylcyclohexyl)phenyl]piperazine methanesulfonic acid salt
CAS No.:894776-31-9
Molecular Formula:CH₄O₃S*C₂₀H₃₂N₂
Molecular Weight:396.594
Hs Code.:

Synonyms:1-[2-(3,3,5,5-tetramethylcyclohexyl)phenyl]piperazine methanesulfonic acid salt

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Chemical Property of 1-[2-(3,3,5,5-tetramethylcyclohexyl)phenyl]piperazine methanesulfonic acid salt

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Technology Process of 1-[2-(3,3,5,5-tetramethylcyclohexyl)phenyl]piperazine methanesulfonic acid salt

There total 2 articles about 1-[2-(3,3,5,5-tetramethylcyclohexyl)phenyl]piperazine methanesulfonic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 894776-24-0
2-(3,3,5,5-tetramethylcyclohexyl)phenylaniline

: 821-48-7
bis-(2-chloroethyl)amine hydrochloride

: 894776-31-9
1-[2-(3,3,5,5-tetramethylcyclohexyl)phenyl]piperazine methanesulfonic acid salt

Guidance literature:: With sodium hydroxide; methanesulfonic acid; sodium chloride; In n-heptane; 4-methylisopropylbenzene; ethyl acetate; toluene;

Reference yield:

: 75-75-2,98527-29-8
methanesulfonic acid

: 894776-24-0
2-(3,3,5,5-tetramethylcyclohexyl)phenylaniline

: 894776-31-9
1-[2-(3,3,5,5-tetramethylcyclohexyl)phenyl]piperazine methanesulfonic acid salt

Guidance literature:: 2-(3,3,5,5-tetramethylcyclohexyl)phenylaniline; bis-(2-chloroethyl)amine hydrochloride; In cymene, p-; at 180 ℃; for 8.5h;

With sodium hydroxide; In cymene, p-; water; at 20 ℃;

methanesulfonic acid; In cymene, p-; ethyl acetate; at 20 ℃; for 1h;

Reference yield:

: 894776-31-9
1-[2-(3,3,5,5-tetramethylcyclohexyl)phenyl]piperazine methanesulfonic acid salt

: 108-10-1
4-methyl-2-pentanone

: 1489-69-6
Cyclopropanecarboxaldehyde

: ER-339093-13

Guidance literature:: With sodium hydroxide; methanesulfonic acid; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; n-heptane; tert-butyl methyl ether;