tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)-1-oxidopyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate

Base Information

Chemical Name:tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)-1-oxidopyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate
CAS No.:1056555-32-8
Molecular Formula:C₄₁H₅₅Cl₂N₃O₁₀S
Molecular Weight:852.874
Hs Code.:

tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)-1-oxidopyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate

Synonyms:tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)-1-oxidopyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate

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Chemical Property of tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)-1-oxidopyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate

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Technology Process of tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)-1-oxidopyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate

There total 10 articles about tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)-1-oxidopyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1056555-30-6
tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)pyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate

: 1056555-32-8
tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)-1-oxidopyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate

Guidance literature:: tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)pyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 18h;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: 921630-61-7
4-[2-(2,6-dichloro-4-methyl-phenoxy)-ethoxy]-benzaldehyde

: 1056555-32-8
tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)-1-oxidopyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate

Guidance literature:: Multi-step reaction with 7 steps

1.1: piperidine / toluene / 3 h / Heating / reflux

2.1: sodium tetrahydroborate; cobalt(II) chloride / tetrahydrofuran; methanol / 2 h / 20 °C

3.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 20 °C

4.1: methanol; sodium hydroxide; water / tetrahydrofuran / 18 h / 20 °C

4.2: pH ~ 1

5.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 18 h / 20 °C

6.1: Oxone / tetrahydrofuran; methanol; water / 2 h / 2 °C

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 18 h / 20 °C

With piperidine; methanol; dmap; Oxone; sodium hydroxide; sodium tetrahydroborate; water; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; HATU; cobalt(II) chloride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1056555-04-4
3-[(tert-butoxycarbonyl)amino]-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}propanoic acid

: 1056555-32-8
tert-butyl (3-(cyclopropyl((2-(3-methoxypropyl)-6-(3-(methylsulfonyl)propoxy)-1-oxidopyridin-4-yl)methyl)amino)-2-(4-(2-(2,6-dichloro-4-methylphenoxy)ethoxy)benzyl)-3-oxopropyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 18 h / 20 °C

2: Oxone / tetrahydrofuran; methanol; water / 2 h / 2 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 18 h / 20 °C

With Oxone; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; HATU; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;