methyl (Z)-3-<3-<4-(3-hydroxy-1-propenyl)phenoxy>-4-methoxyphenyl> propionate

Base Information

Chemical Name:methyl (Z)-3-<3-<4-(3-hydroxy-1-propenyl)phenoxy>-4-methoxyphenyl> propionate
CAS No.:143551-93-3
Molecular Formula:C₂₀H₂₂O₅
Molecular Weight:342.392
Hs Code.:

Synonyms:methyl (Z)-3-<3-<4-(3-hydroxy-1-propenyl)phenoxy>-4-methoxyphenyl> propionate

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Chemical Property of methyl (Z)-3-<3-<4-(3-hydroxy-1-propenyl)phenoxy>-4-methoxyphenyl> propionate

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Technology Process of methyl (Z)-3-<3-<4-(3-hydroxy-1-propenyl)phenoxy>-4-methoxyphenyl> propionate

There total 26 articles about methyl (Z)-3-<3-<4-(3-hydroxy-1-propenyl)phenoxy>-4-methoxyphenyl> propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 143551-92-2
methyl-3-<4-methoxy-<3-<4-(2-(hydroxymethyl)ethynyl)phenoxy>phenyl>>propanoate

: 143551-93-3
methyl (Z)-3-<3-<4-(3-hydroxy-1-propenyl)phenoxy>-4-methoxyphenyl> propionate

Guidance literature:: With hydrogen; Lindlar's catalyst;
DOI:10.1016/S0040-4039(00)74692-2

Reference yield: 94.0%

: 168135-09-9
methyl (Z)-3-<3-<4-(3-t-butyldimethylsilylether-1-propenyl)phenoxy>-4-methoxyphenyl> propionate

: 143551-93-3
methyl (Z)-3-<3-<4-(3-hydroxy-1-propenyl)phenoxy>-4-methoxyphenyl> propionate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1080/00397919508015470

Reference yield:

: 100-00-5
4-chlorobenzonitrile

: 143551-93-3
methyl (Z)-3-<3-<4-(3-hydroxy-1-propenyl)phenoxy>-4-methoxyphenyl> propionate

Guidance literature:: Multi-step reaction with 8 steps

2: 80 percent / pyridine, piperidine

3: 85 percent / H₂ / 10 percent Pd/C

4: H₂SO₄, NaNO₂ / 5 °C

5: KI

6: 96 percent / K₂CO₃ / acetone

7: 56 percent / (PPh₃)2PdCl₂, CuI, Et₃N

8: 95 percent / H₂ / Pd-CaCO₃

With piperidine; pyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sulfuric acid; hydrogen; potassium carbonate; triethylamine; potassium iodide; sodium nitrite; palladium on activated charcoal; Lindlar's catalyst; In acetone;
DOI:10.1016/S0040-4039(00)74692-2