[2-(2-chloro-5-methoxy-4-nitro-phenyl)-ethyl]-(2,4-dimethoxy-benzyl)-amine

Base Information

Chemical Name:[2-(2-chloro-5-methoxy-4-nitro-phenyl)-ethyl]-(2,4-dimethoxy-benzyl)-amine
CAS No.:1437717-45-7
Molecular Formula:C₁₈H₂₁ClN₂O₅
Molecular Weight:380.828
Hs Code.:

Synonyms:[2-(2-chloro-5-methoxy-4-nitro-phenyl)-ethyl]-(2,4-dimethoxy-benzyl)-amine

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Chemical Property of [2-(2-chloro-5-methoxy-4-nitro-phenyl)-ethyl]-(2,4-dimethoxy-benzyl)-amine

Chemical Property:

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Technology Process of [2-(2-chloro-5-methoxy-4-nitro-phenyl)-ethyl]-(2,4-dimethoxy-benzyl)-amine

There total 4 articles about [2-(2-chloro-5-methoxy-4-nitro-phenyl)-ethyl]-(2,4-dimethoxy-benzyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.2%

: 20781-20-8
2,4-Dimethoxybenzylamine

: 1349744-81-5
1-chloro-4-methoxy-5-nitro-2-vinylbenzene

: 1437717-45-7
[2-(2-chloro-5-methoxy-4-nitro-phenyl)-ethyl]-(2,4-dimethoxy-benzyl)-amine

Guidance literature:: With quinoline; In isopropyl alcohol; at 70 ℃; for 20h;

Reference yield:

: 1027833-17-5
1-bromo-2-chloro-5-fluoro-4-nitrobenzene

: 1437717-45-7
[2-(2-chloro-5-methoxy-4-nitro-phenyl)-ethyl]-(2,4-dimethoxy-benzyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 0 °C

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / propan-1-ol / 4 h / Reflux

3: quinoline / isopropyl alcohol / 20 h / 70 °C

With quinoline; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine; In propan-1-ol; isopropyl alcohol;

Reference yield:

: 201849-15-2
2-bromo-1-chloro-4-fluoro-benzene

: 1437717-45-7
[2-(2-chloro-5-methoxy-4-nitro-phenyl)-ethyl]-(2,4-dimethoxy-benzyl)-amine

Guidance literature:: Multi-step reaction with 4 steps

1: potassium nitrate; sulfuric acid / -5 °C / Cooling with ice

2: 0 °C

3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / propan-1-ol / 4 h / Reflux

4: quinoline / isopropyl alcohol / 20 h / 70 °C

With quinoline; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sulfuric acid; potassium nitrate; triethylamine; In propan-1-ol; isopropyl alcohol;