benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate

Base Information

Chemical Name:benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate
CAS No.:911229-06-6
Molecular Formula:C₁₉H₂₁NO₆
Molecular Weight:359.379
Hs Code.:

Synonyms:benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate

Suppliers and Price of benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate

Chemical Property:

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Technology Process of benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate

There total 1 articles about benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2033-24-1
cycl-isopropylidene malonate

: 19099-93-5
benzyl 4-oxo-1-piperidinecarboxylate

: 911229-06-6
benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate

Guidance literature:: With piperidine; pyridine; at 20 - 45 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.04.094

Reference yield:

: 911229-06-6
benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate

: 90878-19-6
phenethylmagnesium chloride

: C₂₇H₃₁NO₆

Guidance literature:: phenethylmagnesium chloride; With copper(l) iodide; In tetrahydrofuran; at -10 ℃; for 0.5h; Inert atmosphere;

benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate; In tetrahydrofuran; at -10 - 0 ℃; for 4h;
DOI:10.1016/j.tet.2009.04.094

Reference yield:

: 911229-06-6
benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate

: 100-58-3
phenylmagnesium bromide

: C₂₅H₂₇NO₆

Guidance literature:: phenylmagnesium bromide; With copper(l) iodide; In tetrahydrofuran; at -10 ℃; for 0.5h; Inert atmosphere;

benzyl 4-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)piperidine-1-carboxylate; In tetrahydrofuran; at -10 - 0 ℃; for 4h;
DOI:10.1016/j.tet.2009.04.094