N,N'-(naphthalene-1,4-diyl)bis(4-chlorobenzenesulfonamide)

Base Information

• Chemical Name: N,N'-(naphthalene-1,4-diyl)bis(4-chlorobenzenesulfonamide)
• CAS No.: 167321-72-4
• Molecular Formula: C₂₂H₁₈N₂O₄S₂
• Molecular Weight: 438.528
• Mol file: 167321-72-4.mol

Synonyms:N,N'-(naphthalene-1,4-diyl)bis(4-chlorobenzenesulfonamide)

Chemical Property of N,N'-(naphthalene-1,4-diyl)bis(4-chlorobenzenesulfonamide)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-(naphthalene-1,4-diyl)bis(4-chlorobenzenesulfonamide)

There total 8 articles about N,N'-(naphthalene-1,4-diyl)bis(4-chlorobenzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1,4-diaminonaphthalene (2243-61-0) + benzenesulfonyl chloride (98-09-9) → N,N'-(naphthalene-1,4-diyl)bis(4-chlorobenzenesulfonamide) (167321-72-4)

Guidance literature:

With pyridine; at 20 ℃; for 2h;

DOI:10.1080/10715762.2020.1732955

Reference yield: 51.0%

(4-amino-1-naphthyl)amine dihydrochloride + benzenesulfonyl chloride (98-09-9) → N,N'-(naphthalene-1,4-diyl)bis(4-chlorobenzenesulfonamide) (167321-72-4)

Guidance literature:

With pyridine; at 20 ℃; for 24h;

DOI:10.1016/j.ejmech.2015.08.049

Reference yield:

N,N'-bis(phenylsulfonyl)-1,4-naphthoquinone diimine (42976-05-6,83202-22-6) → N,N'-(naphthalene-1,4-diyl)bis(4-chlorobenzenesulfonamide) (167321-72-4)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether; benzene;

DOI:10.1021/ja01108a045

upstream raw materials:

1-acetoxybuta-1,3-diene

N,N'-bis(phenylsulfonyl)-p-benzoquinone diimine

N,N'-bis(phenylsulfonyl)-1,4-naphthoquinone diimine

benzenesulfonyl chloride

Downstream raw materials:

N,N'-bis(phenylsulfonyl)-1,4-naphthoquinone diimine

N,N'-(2-chloro-naphthalene-1,4-diyl)-bis-benzenesulfonamide