N,N'-bis(phenylsulfonyl)-1,4-naphthoquinone diimine

Base Information

• Chemical Name: N,N'-bis(phenylsulfonyl)-1,4-naphthoquinone diimine
• CAS No.: 42976-05-6
• Molecular Formula: C₂₂H₁₆N₂O₄S₂
• Molecular Weight: 436.512
• Mol file: 42976-05-6.mol

Synonyms:

Chemical Property of N,N'-bis(phenylsulfonyl)-1,4-naphthoquinone diimine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N'-bis(phenylsulfonyl)-1,4-naphthoquinone diimine

There total 5 articles about N,N'-bis(phenylsulfonyl)-1,4-naphthoquinone diimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

N,N'-(naphthalene-1,4-diyl)bis(4-chlorobenzenesulfonamide) (167321-72-4) → N,N'-bis(phenylsulfonyl)-1,4-naphthoquinone diimine (42976-05-6,83202-22-6)

Guidance literature:

With chloramine-B; In ethanol; for 2h;

Reference yield: 90.0%

1,4-bis(phenylsulfonylamino)tetralin (76353-03-2) → N,N'-bis(phenylsulfonyl)-1,4-naphthoquinone diimine (42976-05-6,83202-22-6)

Guidance literature:

With lead(IV) acetate; In acetic acid; at 30 - 50 ℃; for 2h;

Reference yield:

benzenesulfonyl chloride (98-09-9) → N,N'-bis(phenylsulfonyl)-1,4-naphthoquinone diimine (42976-05-6,83202-22-6)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; benzene

2: lead (IV)-acetate

With pyridine; lead(IV) acetate; benzene;

DOI:10.1021/ja01145a048

upstream raw materials:

N,N'-(naphthalene-1,4-diyl)bis(4-chlorobenzenesulfonamide)

1,4-bis(phenylsulfonylamino)tetralin

tetralin

benzenesulfonamide sodium salt

Downstream raw materials:

N,N'-(1,4-dihydro-anthracene-9,10-diyl)-bis-benzenesulfonamide

N,N'-((E,E)-1a,2,7,7a-tetrahydro-spiro[cyclopropa[b]naphthalene-1,9'-fluorene]-2,7-diylidene)-bis-benzenesulfonamide

1,3,2-Naphthoazathiaphosphol-1,5-bis(benzenesulfonamido)-2(4-methoxyphenyl)-2-sulfide